1,720,997 research outputs found
Additive Manufacturing of AlSi10Mg and Ti6Al4V Lightweight Alloys via Laser Powder Bed Fusion: A Review of Heat Treatments Effects
Effect of surface roughness and industrial heat treatments on the microstructure and mechanical properties of Ti6Al4V alloy manufactured by laser powder bed fusion in different built orientations
The emergence of powder bed fusion in recent years has made it one of the most demanded additive manufacturing technologies for Ti6Al4V alloys in the biomedical and aerospace industries due to its ease of part fabrication with complex geometry. However, Ti6Al4V components require a post-processing treatment to optimize their mechanical properties for engineering applications. The present study offers an analysis of the effects of different industrial heat treatments (704 °C for 120 min, 740 °C for 130 min) on the microstructure and tensile properties of Ti6Al4V samples manufactured by laser powder bed fusion in different orientations (Z, 45°, XY and XZ). These heat treatments were selected to improve the mechanical properties of the as-built material and to obtain samples representative of real industrial applications. SEM observations illustrated that the α’ martensite grown in the columnar parent β-grains was converted into an α+β mixture after both heat treatments. EBSD showed that the newly formed α phase maintained, inside the parent β grains, the same orientation relationship as the as-built α′ martensite. However, on a macroscopic scale, the α phase exhibited no preferential orientation. The heat-treated samples, which exhibited approximately 10% lower ultimate tensile strength and yield strength than the as built samples but a 10–13% higher elongation, were practically isotropic in their mechanical response. What little anisotropy was left was mainly attributed to few elongated interlamellar pores. The sandblasting process was also investigated; it did not affect the static mechanical properties of the samples but it reduced the Ra values by 25%. Finally, Vickers microhardness vs. strength relationships were studied by considering the α-phase orientation
Defect-Correlated Vickers Microhardness of Al-Si-Mg Alloy Manufactured by Laser Powder Bed Fusion with Post-process Heat Treatments
Laser powder bed fusion is an additive manufacturing process characterized by different advantages like the manufacture of samples with complex geometry without the use of tools and/or molds. Generally, the manufactured samples are characterized by high tensile strengths which, however, can be affected by the presence of defects due to the unoptimized process parameters. In a large applications field, a low density of the as-built AlSi10Mg samples is a very important parameter to considered, e.g., due to both the loss of the tensile strengths correlated with a premature failure of the samples and the increase in time and costs associated with the manufacturing process. In addition, different post-process heat treatments can increase these effects leading to an ineffective manufacturing process. In this scenario, the present work shows the analysis of spherical and lack-of-fusion pores induced by the laser powder bed fusion process on the AlSi10Mg samples and their variations after different heat treatments (direct aging and T6). At the same time, the influence of pores on the Vickers microhardness and the tensile properties has been studied in the same AlSi10Mg samples (bars and billets) that were printed with single- and double-laser machine setup. Different process parameters were also analyzed and compared. The study was supported by the microstructural and pore analysis performed by optical microscopy along the XZ plane (build direction) and the XY plane. Finally, the greatest effects of pores were observed on the Vickers microhardness values; in fact, two different relationships between microhardness and density variation are discussed. The T6 heat treatment leads to a rounding of the pores already formed in the as-built samples and to a formation of new small pores. Graphical Abstract: [Figure not available: see fulltext.
Ti6Al4V-ELI Alloy Manufactured via Laser Powder-Bed Fusion and Heat-Treated below and above the β-Transus: Effects of Sample Thickness and Sandblasting Post-Process
Ti6Al4V-ELI is the most-used lightweight alloy in the aerospace industrial sector thanks to its high mechanical strength and corrosion resistance. The present paper aims, firstly, to evaluate the effects induced by different heat treatments, which were performed above and below the β-transus temperature on Ti6Al4V-ELI samples manufactured via Laser Powder-Bed Fusion in different orienta-tions (XZ, XY, Z and 45◦ ). The first set of tensile samples and bars were heat-treated at 1050◦ C × 1 h, while the second and third set were heat-treated at 704◦ C × 120′ following the AMS2801 standard specification, and at 740◦ C × 130′ . These heat treatments were chosen to improve the as-built mechanical properties according to the ASTM F3001 and also ASTM F2924-14 standard specifications. Optical and SEM measurements reveal primary, secondary and tertiary α-laths below the β-transus, while above this temperature, the microstructure varies in relation to the sample’s thickness. Secondly, this work analyzed the results obtained after a sandblasting process, which was performed on half of all the available heat-treated tensile samples, through XRD and Vickers microhardness measurements. XRD analysis also highlighted the presence of α2-Ti3 Al and TiAl3 precipitates and the microstructural change in terms of the α-phase
Effect of the Distance from Build Platform and Post-Heat Treatment of AlSi10Mg Alloy Manufactured by Single- and Multi-Laser Selective Laser Melting
In the present study, AlSi10Mg samples produced by selective laser melting (SLM) were studied. Samples were machined from two types of bars obtained through different methods: either single laser (SL) or multiple laser (ML) machine setup. The bars were built perpendicular to the platform, which was pre-heated at 150 °C (working temperature), up to a height of 300 mm. The effect of the distance from the platform on the mechanical properties was investigated through tensile samples in as-built condition and after unconventional heat treatments (U-HT). Tensile strength changed by 80 MPa along the Z-axis (build direction) for SL case and by 100 MPa for ML case in the as-built samples. Vickers microhardness revealed an analogous gradient. This was correlated to a gradient in intra-granular precipitates' distribution along the Z-axis, as revealed by scanning electron microscopy (SEM). An unconventional heat treatment at 175 °C for 6h slightly improves the mechanical strength; higher temperature treatments at 200 and 225 °C for the same duration cause a progressive decrease in strength with an increase in elongation. The amount and size of the precipitates and the thickness of eutectic Si change with the heat treatment temperature, justifying the mechanical behavior
Work hardening of heat-treated alsi10mg alloy manufactured by single and double laser selective laser melting: Effects of layer thickness and hatch spacing
The present study analyzed the microstructure and the mechanical properties of AlSi10Mg SLMed bars (10 × 10 × 300 mm) and billets (10 × 100 × 300 mm) before and after the direct aging at 200 °C for 4 h and the T6 heat treatment. The discussed results are compared to those obtained by the AlSi10Mg samples manufactured with the same geometry but using different process parameters (layer thickness higher than 40 μm and a hatch spacing lower than 100 μm) and also through the Quality Index (QI). These work conditions allow the obtaining of a microstructural variation and different tensile properties in as-built top samples. In both batches, the cycle time was 45 h and together with the preheated build platform at 150 °C, induced an increase of UTS (Ultimate Tensile Strength) and yield strength on the bottom rather than the top samples due to the aging phenomena. Upon completion of the direct aging heat treatment, the effects induced by the platform were can-celled, keeping a full cellular microstructure that characterized the as-built SLMed (Selective Laser Melted) samples. Moreover, the Considère criterion and the work hardening analysis showed that the failure occurs after the necking formation in some of the T6 heat-treated samples. In this last case, the Si eutectic network globularized into Si particles, causing a decrease of UTS (from around 400 MPa to 290 MPa) in favour of an increase of ductility up to 15% and reaching a QI in the range 400 ÷ 450 MPa. These values place these samples between the high-quality aluminium cast alloy and T6 heat-treated ones
Tracing and attaching bank accounts in EU cross-border insolvency proceedings
Tracing and attaching bank accounts (“TAB”) is complex in cross-border insolvency
situations. The paper tackles such complexities and spells out the instruments that insolvency
practitioners may use in the EU context. Accordingly, the author dwells primarily on Regulation (EU)
2015/848 to detect the extraterritorial powers it confers to insolvency practitioners and explain how it
governs the coordination between the lex concursus and the law of the State where the bank account is
located when it comes to determining practicable attachment measures. The paper also clarifies when
insolvency practitioners may resort to the European Account Preservation Order (EAPO) as an
alternative pathway to national measures. Four special focuses conclude the analysis. The first concerns
the future of EU harmonisation in TAB activity; the second compares intra and extra-EU TAB
operations; the third and fourth examine the restrictions on TAB measures flowing from sovereign bank
accounts and accounts frozen because of economic sanctions
Going Beyond Counting First Authors in Author Co-citation Analysis
The present study examines one of the fundamental aspects of author co-citation analysis (ACA) - the way co-citation
counts are defined. Co-citation counting provides the data on which all subsequent statistical analyses and mappings
are based, and we compare ACA results based on two different types of co-citation counting - the traditional type that
only counts the first one among a cited work's authors on the one hand and a non-traditional type that takes into
account the first 5 authors of a cited work on the other hand. Results indicate that the picture produced through this non-traditional author co-citation counting contains more coherent author groups and is therefore considerably clearer. However, this picture represents fewer specialties in the research field being studied than that produced through the traditional first-author co-citation counting when the same number of top-ranked authors is selected and analyzed. Reasons for these effects are discussed
Aging Profiles of AlSi7Mg0.6 and AlSi10Mg0.3 Alloys Manufactured via Laser-Powder Bed Fusion: Direct Aging versus T6
The artificial aging heat treatments performed directly on as-built and solubilized AlSi7Mg0.6 and AlSi10Mg0.3 samples were characterized and discussed. The analysed bars and billets (height of 300 mm) were manufactured via the Laser Powder-Bed Fusion process on a build platform heated at 150 °C. Therefore, its influence on the as-built samples was studied in terms of mechanical performance variations between the bottom and top regions. Vickers microhardness measurements were performed to obtain aging profiles after direct aging (175–225 °C) and T6 heat treatments and to highlight better time and temperature parameters to optimize the mechanical properties of both alloys. SEM observations were used to characterize the microstructure before and after the heat treatments and its influence on the fracture mechanisms. Generally, the direct aging heat treatments show the same effects on both aluminium alloys, unlike the solubilization at 505 °C followed by artificial aging at 175 °C. The strengths vs. elongation values obtained after the direct aging treatments are better than those exhibited by T6 as highlighted by the quality index
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