1,720,964 research outputs found
Phase-shifting-holography software package
No full textSoftware package for phase shifting off axis holograph
Langmuir analysis of electron beam induced plasma in environmental TEM
No full textThe characterisation of the gas state under electron impact is of high importance for the understanding of materials in-situ environmental transmission electron microscopy (ETEM) experiments. We report on the formation of a dilute plasma state of Ar and He based on the development of a Langmuir probe as a plasma diagnostic tool for the differentially pumped volume at the TEM sample position in the octagon. In order to keep stray magnetic field influences of the objective lens small, and thus the results readily interpretable within existing theory, the experiments are performed in Lorentz mode. The applicability of Langmuir type analysis for the identification of plasma parameters, such as ion density, plasma temperature, sheath extension and electron energy distribution is examined. The systematic study as a function of gas pressure and beam current reveals cold plasma characteristics with electron temperatures of around 0.4 eV and ion and electron densities that are orders of magnitude below the expected values from ionisation cross sections. The loss of charged particles appears to be due to surface collisions at the electrically conducting pole piece surfaces as well as at the conductive parts of the TEM holder
Going Beyond Counting First Authors in Author Co-citation Analysis
Full text linkThe present study examines one of the fundamental aspects of author co-citation analysis (ACA) - the way co-citation
counts are defined. Co-citation counting provides the data on which all subsequent statistical analyses and mappings
are based, and we compare ACA results based on two different types of co-citation counting - the traditional type that
only counts the first one among a cited work's authors on the one hand and a non-traditional type that takes into
account the first 5 authors of a cited work on the other hand. Results indicate that the picture produced through this non-traditional author co-citation counting contains more coherent author groups and is therefore considerably clearer. However, this picture represents fewer specialties in the research field being studied than that produced through the traditional first-author co-citation counting when the same number of top-ranked authors is selected and analyzed. Reasons for these effects are discussed
Atom Surface Dynamics of Manganese Oxide under Oxygen Evolution Reaction-Like Conditions Studied by In Situ Environmental Transmission Electron Microscopy
No full textHydrogen production by electrochemical water splitting is limited by the sluggish oxygen evolution reaction (OER). In order to improve our understanding of the underlying mechanisms, information about the atomic surface structure of the active state of the electrode is required. Here, we present environmental transmission electron microscopy studies of Ca-birnessite (K0.20Ca0.21MnO2.21·1.4H2O) electrodes under conditions close to those of the OER. Remarkably, in H2O vapor, a highly dynamic state of the surface and subsurface develops with a thickness of the formed dynamic layer of up to 0.6 nm, which is absent in O2 and inert gases. Electron beam-induced effects are carefully studied, showing high stability of the material against radiation damage in high vacuum until a dose rate of 42,000 e–/(Å2 s). In contrast, in H2O, the dynamic surface layer develops and forms a stationary state even at low dose rates, down to 5000 e–/(Å2 s). Electron energy-loss spectroscopy reveals an increase in the Mn oxidation state in H2O and in O2 ambient. Our results are interpreted as the formation of a few-angstrom-thick, dynamic, and hydrated surface layer of birnessite in H2O, with an increased Mn valence state. Such a dynamic surface layer with a flexible Mn coordination and valence state might be optimal for oxygen evolution due to the higher effective interaction volume beyond the surface area and a flexible bond coordination of partially hydrated Mn species
Variations on the Author
Full text link“Variations on the Author” discusses two of Eduardo Coutinho’s recent films (Um Dia na Vida, from 2010, and Últimas Conversas, posthumously released in 2015) and their contribution to the general question of documentary authorship. The director’s filmography is characterized by a consistent yet self-effacing form of authorial self-inscription: Coutinho often features as an interviewer that rather than express opinions propels discourses; an interviewer that is good at listening. This mode of self-inscription characterizes him as an author who is not expressive but who is nonetheless markedly present on the screen. In Um Dia na Vida, however, Coutinho is completely absent form the image, while Últimas Conversas, on the contrary, includes a confessional prologue that moves the director from the margins to the center of his films. This article examines the ways in which these works stand out in the filmography of a director who offers new insights into the notion of cinematic authorship
Appropriate Similarity Measures for Author Cocitation Analysis
Full text linkWe provide a number of new insights into the methodological discussion about author cocitation analysis. We first argue that the use of the Pearson correlation for measuring the similarity between authors’ cocitation profiles is not very satisfactory. We then discuss what kind of similarity measures may be used as an alternative to the Pearson correlation. We consider three similarity measures in particular. One is the well-known cosine. The other two similarity measures have not been used before in the bibliometric literature. Finally, we show by means of an example that our findings have a high practical relevance.information science;Pearson correlation;cosine;similarity measure;author cocitation analysis
Dispelling the Myths Behind First-author Citation Counts
Full text linkWe conducted a full-scale evaluative citation analysis study of scholars in the XML research field to explore just how different from each other author rankings resulting from different citation counting methods actually are, and to demonstrate the capability of emerging data and tools on the Web in supporting more realistic citation counting methods. Our results contest some common arguments for the continued
use of first-author citation counts in the evaluation of scholars, such as high correlations between author rankings by first-author citation counts and other citation
counting methods, and high costs of using more realistic citation counting methods that are not well-supported by the ISI databases. It is argued that increasingly available digital full text research papers make it possible for citation analysis studies to go beyond what the ISI databases have directly supported and to employ more
sophisticated methods
koamabayili/VECTRON-author-checklist: VECTRON author checklist
No full textWe have done our best to complete the author checklist relating to the use of animals in the hut study. Note that the objective for the hut study was to evaluate the IRS treatment applications for residual efficacy against Anopheles mosquitoes, including the local An. coluzzii mosquito population. Cows were only used to attract mosquitoes into the huts and no tests were carried out directly on the cows. The author checklist is intended for use with studies where experiments are carried out on animals, which is why we have had such difficulty in completing this for the hut study, as many of the questions do not relate to how the cows were used
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