1,721,010 research outputs found
A Dedicated Endstation for Waveguide-based X-Ray Imaging
No full textSoftcover, 17x24X-ray microscopy has emerged as a powerful and versatile imaging technique in many fields of science over the last years, offering insights in opaque media at high spatial resolution. A major challenge remains the fabrication of suitable X-ray lenses, e.g., Fresnel zone plates or compound refractive lenses. In an alternative approach of a lensless imaging scheme the sample is illuminated by a coherent X-ray beam. The sample information is then reconstructed from the recorded diffraction signal by numerical iterative algorithms. Within this thesis the basics of lensless holographic imaging with X-Ray waveguides are summarised and extended to the concept of waveguide-based X-ray interferometry. The specific instrumentation required for the conceptual experiments of waveguide-based holographic imaging is explained and illustrated by the obtained results. Based on the results of these conceptual experiments a dedicated synchrotron endstation for waveguide-based holographic imaging was designed and built. The specifications and properties of the Kirkpatrick-Baez focussing mirrors and other mechanical and optical components are described in detail, along with the instrument control system and various available detectors. First commissioning results prove the imaging abilities of the presented endstation
Coherent propagation of white X-rays in a planar waveguide
No full textThe far-field diffraction pattern of a front-coupled planar waveguide supporting two guided modes has been measured using a white X-ray beam. Interference of the guided modes leads to a characteristic variation of the far-field diffraction pattern for different photon energies. The experiment verifies the predicted properties of the guided modes, shows that these modes superpose coherently, and demonstrates that the electromagnetic field downstream of the waveguide is significantly different from that expected for a hypothetical small slit of the same size
Object localization with 10nm accuracy by x-ray phase contrast projection imaging
No full textThe present work focuses on the question of localizing single object by hard x-ray phase contrast projection imaging. The authors present a setup where an x-ray channel waveguide defines a "quasi-point source" used to illuminate and image an object in a highly coherent cone beam. Knife edge fluorescence scans revealed a beam diameter of 75 nm at a distance of 30 mu m behind the guide. The recorded image corresponds to an in-line hologram of the object which can be reconstructed numerically. Object translations and associated shifts in the hologram allow for the 10 nm localization accuracy. (c) 2007 American Institute of Physics
Highly sensitive quantitative biological imaging by scanning X-ray diffraction microscopy
No full textFocus characterization of the NanoMAX Kirkpatrick–Baez mirror system
No full textThe focusing and coherence properties of the NanoMAX Kirkpatrick–Baez mirror system at the fourth-generation MAX IV synchrotron in Lund have been characterized. The direct measurement of nano-focused X-ray beams is possible by scanning of an X-ray waveguide, serving basically as an ultra-thin slit. In quasi-coherent operation, beam sizes of down to 56 nm (FWHM, horizontal direction) can be achieved. Comparing measured Airy-like fringe patterns with simulations, the degree of coherence |μ| has been quantified as a function of the secondary source aperture (SSA); the coherence is larger than 50% for SSA sizes below 11 µm at hard X-ray energies of 14 keV. For an SSA size of 5 µm, the degree of coherence has been determined to be 87%
Holographic and diffractive x-ray imaging using waveguides as quasi-point sources
No full textWe report on lensless nanoscale imaging using x-ray waveguides as ultra-small sources for quasi-point-like illumination. We first give a brief account of the basic optical setup, an overview of the progress in waveguide fabrication and characterization, as well as the basics of image formation. We then compare one-step holographic and iterative ptychographic reconstruction, both for simulated and experimental data collected on samples illuminated by waveguided beams. We demonstrate that scanning the sample with partial overlap can substantially improve reconstruction quality in holographic imaging, and that divergent beams make efficient use of the limited dynamic range of current detectors, regardless of the reconstruction scheme. Among different experimental settings presented, smallest source dimensions of 29 nm (horizontal) x 17 nm have been achieved, using multi-modal interference effects. These values have been determined by ptychographic reconstruction of a Ta test structure at 17.5 keV and have been corroborated by simulations of field propagation inside the waveguide
Versatility of a hard X-ray Kirkpatrick-Baez focus characterized by ptychography
No full textIn the past decade Kirkpatrick-Baez (KB) mirrors have been established as powerful focusing systems in hard X-ray microscopy applications. Here a ptychographic characterization of the KB focus in the dedicated nano-imaging setup GINIX (Göttingen Instrument for Nano-Imaging with X-rays) at the P10 coherence beamline of the PETRA III synchrotron at HASLYLAB/DESY, Germany, is reported. More specifically, it is shown how aberrations in the KB beam, caused by imperfections in the height profile of the focusing mirrors, can be eliminated using a pinhole as a spatial filter near the focal plane. A combination of different pinhole sizes and illumination conditions of the KB setup makes the prepared optical setup well suited not only for high-resolution ptychographic coherent X-ray diffractive imaging but also for moderate-resolution/large-field-of-view propagation imaging in the divergent KB beam
Sub-15 nm beam confinement by two crossed x-ray waveguides
No full textWe have combined two high transmission planar x-ray waveguides glued onto each other in a crossed geometry to form an effective quasi-point source. From measurements of the far-field diffraction pattern, the phase and amplitude of the near-field distribution is retrieved using the error-reduction algorithm. In agreement with finite difference field simulations (forward calculation), the reconstructed exit wave intensity distribution (inverse calculation) exhibits a full width at half maximum (FWHM) below 15 nm in both dimensions. Finally, holographic imaging is successfully demonstrated for the crossed waveguide device by translation of a lithographic test structure through the waveguide beam. (C) 2010 Optical Society of Americ
Compound focusing mirror and X-ray waveguide optics for coherent imaging and nano-diffraction
No full textA compound optical system for coherent focusing and imaging at the nanoscale is reported, realised by high-gain fixed-curvature elliptical mirrors in combination with X-ray waveguide optics or different cleaning apertures. The key optical concepts are illustrated, as implemented at the Göttingen Instrument for Nano-Imaging with X-rays (GINIX), installed at the P10 coherence beamline of the PETRA III storage ring at DESY, Hamburg, and examples for typical applications in biological imaging are given. Characteristic beam configurations with the recently achieved values are also described, meeting the different requirements of the applications, such as spot size, coherence or bandwidth. The emphasis of this work is on the different beam shaping, filtering and characterization methods
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