562,503 research outputs found

    Phase behaviour and crystal structures of 2′,3′-difluorinated p-terphenyl derivatives

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    The crystal structures of difluorine derivatives of p-terphenyls (nTm) have been determined by single-crystal X-ray diffraction. For the unsymmetrical substituted compounds 2′,3′-difluoro-4-methyl-p-terphenyl (1T0, C19H14F2) and 4-ethyl-2′,3′-difluoro-4′′-methyl-p-terphenyl (1T2, C21H18F2), the crystal structure is disordered, with molecules statistically entering the crystal in up and down orientations, with full superposition of all the atoms, except for those of the terminal groups (H/methyl for 1T0 and methyl/ethyl for 1T2). For triclinic 2′,3′-difluoro-4,4′′-dimethyl-p-terphenyl (1T1, C20H16F2), with the space group P , the two crystallographically independent molecules have the same conformation, which is different from monoclinic 1T0 (space group C2) and 1T2 (space group C2/c). A common feature of the conformation of the three compounds is the noncoplanar twisted arrangement of the three rings of the p-terphenyl moiety. Two-dimensional (2D) Hirshfeld fingerprint plots are consistent with H ... H and C ... H contacts in the crystal packing. For the three compounds, the phase behaviour has been investigated by POM (Petra/Osiris/Molinspiration) and differential scanning calorimetry (DSC) analysis. 1T2 is mesogenic, with enantiotropic nematic behaviour

    Das-1 IgG and IgM recognize a glycosylation epitope.

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    Chemical deglycosylation of the antigen results in near complete loss of signal as measured by western blot analysis using (A) Das-1 IgM and (B) Das-1 IgG. Quantification of band intensity is presented below each band.</p

    Sample ARPES data

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    This is a sample ARPES spectra and Fermi map data acquired by Scienta-Omicron SES program. The spectra is taken on Bi2Se3 sample

    Going Beyond Counting First Authors in Author Co-citation Analysis

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    The present study examines one of the fundamental aspects of author co-citation analysis (ACA) - the way co-citation counts are defined. Co-citation counting provides the data on which all subsequent statistical analyses and mappings are based, and we compare ACA results based on two different types of co-citation counting - the traditional type that only counts the first one among a cited work's authors on the one hand and a non-traditional type that takes into account the first 5 authors of a cited work on the other hand. Results indicate that the picture produced through this non-traditional author co-citation counting contains more coherent author groups and is therefore considerably clearer. However, this picture represents fewer specialties in the research field being studied than that produced through the traditional first-author co-citation counting when the same number of top-ranked authors is selected and analyzed. Reasons for these effects are discussed

    Sample Powder X-ray Diffraction data of CeMg3

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    This sample Powder X-ray Diffraction data of CeMg3 is used for FullProf tutorial https://fullprof.readthedocs.io/ The data file contains 2theta vs intensity data in two column plaintext (.x_y) format

    Nota sobre o "muzimo" do abrigo com pinturas rupestres da Mavita

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    Es separata de: XIII Congresso Luso-Espanhol Para o Progresso das Ciências, 4ª Secçâo, Ciências Naturais, t.VÉ separata de: XIII Congresso Luso-Espanhol Para o Progresso das Ciências, 4ª Secçâo, Ciências Naturais, t.VEn p. 600 se cita una obra de 1950Na p. 600 cítase unha obra de 195

    Sistema automatizado para cultivo de plantas baseado internet das coisas

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    This work consists of developing an indoor greenhouse for growing plants through an automated system using the principle of the internet of things. Using the control of temperature variables, air and soil humidity and luminosity, using sensing connected to the ESP32 platform. The user is given control and access to the status of the greenhouse, providing an environment for quality cultivation and easy construction.Este trabalho consiste no desenvolvimento de uma estufa indoor para o cultivo de plantas por meio de um sistema automatizado utilizando o princípio da internet das coisas. Com o emprego do controle das variáveis de temperatura, umidade do ar e do solo e luminosidade, utilizando o sensoriamento conectado à plataforma ESP32. Proporciona-se ao usuário o controle e acesso ao status da estufa, fornecendo um ambiente para cultivo de qualidade e de fácil construção

    Debendranath-Das/Blockchain-enabled-Multicurrency-Supported-Distributed-e-Banking-System: Initial Release

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    &lt;p&gt;&lt;strong&gt;Full Changelog&lt;/strong&gt;: https://github.com/Debendranath-Das/Blockchain-enabled-Multicurrency-Supported-Distributed-e-Banking-System/commits/v1.0.0&lt;/p&gt

    Appropriate Similarity Measures for Author Cocitation Analysis

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    We provide a number of new insights into the methodological discussion about author cocitation analysis. We first argue that the use of the Pearson correlation for measuring the similarity between authors’ cocitation profiles is not very satisfactory. We then discuss what kind of similarity measures may be used as an alternative to the Pearson correlation. We consider three similarity measures in particular. One is the well-known cosine. The other two similarity measures have not been used before in the bibliometric literature. Finally, we show by means of an example that our findings have a high practical relevance.information science;Pearson correlation;cosine;similarity measure;author cocitation analysis
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