1,721,040 research outputs found

    Identifications of polyphenols and quantification of anthocyanidins in grapes and grape-derived products

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    Polyphenols in grapes and grape-derived products have attracted public and scientific attention due to their numerous protective roles to human health. A rapid and comprehensive qualitative method was developed to characterize the different classes of polyphenols, such as anthocyanins, flavonols, phenolic acids and flavanols/proanthocyanidins, in grapes and grape-derived products. The detection was achieved by two runs with same HPLC gradient in different MS ionization modes and mobile phase modifiers (positive mode and 0.4% trifluoroacetic acid for anthocyanins and flavonols, negative mode and 0.1% formic acid for phenolic acids and flavanols). Under the optimized LC/MS conditions and based on the analysis of the MS and UV data and in comparison with the authenticated standards, a total of 53 polyphenolic compounds were successfully separated and individually identified including 33 anthocyanins, 12 flavonols, 4 phenolic acids and 4 flavanols/proanthocyanidins. With the method developed, a survey was conducted to qualitatively assess and compare the composition of polyphenols among 29 grapes and grape-derived products. To facilitate the quantitation of the major class of polyphenolic anthocyanidins, a simple and precise acid assisted hydrolysis method was established for the quantitation of anthocyanidins in grape juice samples, grape berries and grape skins using LC/MS. Five most common anthocyanidins of delphenidin, petunidin, cyanidin, malvidin, and peonidin in the hydrolyzed grape extracts were included in the quantification study. The validation of this method showed that the recovery percentages of five anthocyanidins ranged from 98.59 % to 103.20% with the relative standard deviation (RSD) less than 5.03%. The qualitative method provided complete insight into the composition of polyphenols in grapes, and other grape-derived products. This quantitative method provides a rapid and accurate tool to quantitatively study individual anthocyanidin in grapes or grape juice samples for quality control and to facilitate the evaluation and comparison of new commercial grapes or grape juice products in market.M.S.Includes bibliographical referencesby Yanping X

    Driving Risk Analysis Based on Driving Experience at Hook-Turn Intersection Using the Emerging Virtual Reality Technology

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    The hook turn, which is rarely seen outside of Melbourne, Australia, reduces congestion in narrow road spaces shared with trams. Australia allows people from 44 nations to convert their home country driver’s license to an Australian driver’s license without a driving test. Visitors who have never heard of the hook-turn experience difficulty driving following the new traffic rule. From this aspect, investigating how inexperienced drivers encounter the hook-turn intersection is valuable for safety reasons. A driving simulator including virtual reality technology is developed to evaluate the level of safety of human driving behavior. The simulator in this research was developed by integrating Vissim and Unity3D embedded head-mounted display and driving devices to ensure a better driving experience. This research presented the development of a robust virtual reality driving simulator. It investigated how nonexperienced drivers respond to a completely new road condition. The results were compared with microsimulation outcomes (here, Vissim). The results showed that a human-driven car had a higher collision risk than a computer-driven car. The trajectories of the driver type were statistically different (t = 6.03, p 0.01, in the case of time-to collision ≤1.5 between experienced and computerized drivers). Participant responses to a postexperiment survey found that the simulator was realistic (4.31 out of 5.00), which could help beginner drivers (4.00 out of 5.00). Therefore, the simulator can be utilized for safety-related research as well as drivers’ training

    Going Beyond Counting First Authors in Author Co-citation Analysis

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    The present study examines one of the fundamental aspects of author co-citation analysis (ACA) - the way co-citation counts are defined. Co-citation counting provides the data on which all subsequent statistical analyses and mappings are based, and we compare ACA results based on two different types of co-citation counting - the traditional type that only counts the first one among a cited work's authors on the one hand and a non-traditional type that takes into account the first 5 authors of a cited work on the other hand. Results indicate that the picture produced through this non-traditional author co-citation counting contains more coherent author groups and is therefore considerably clearer. However, this picture represents fewer specialties in the research field being studied than that produced through the traditional first-author co-citation counting when the same number of top-ranked authors is selected and analyzed. Reasons for these effects are discussed

    Variations on the Author

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    “Variations on the Author” discusses two of Eduardo Coutinho’s recent films (Um Dia na Vida, from 2010, and Últimas Conversas, posthumously released in 2015) and their contribution to the general question of documentary authorship. The director’s filmography is characterized by a consistent yet self-effacing form of authorial self-inscription: Coutinho often features as an interviewer that rather than express opinions propels discourses; an interviewer that is good at listening. This mode of self-inscription characterizes him as an author who is not expressive but who is nonetheless markedly present on the screen. In Um Dia na Vida, however, Coutinho is completely absent form the image, while Últimas Conversas, on the contrary, includes a confessional prologue that moves the director from the margins to the center of his films. This article examines the ways in which these works stand out in the filmography of a director who offers new insights into the notion of cinematic authorship

    Appropriate Similarity Measures for Author Cocitation Analysis

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    We provide a number of new insights into the methodological discussion about author cocitation analysis. We first argue that the use of the Pearson correlation for measuring the similarity between authors’ cocitation profiles is not very satisfactory. We then discuss what kind of similarity measures may be used as an alternative to the Pearson correlation. We consider three similarity measures in particular. One is the well-known cosine. The other two similarity measures have not been used before in the bibliometric literature. Finally, we show by means of an example that our findings have a high practical relevance.information science;Pearson correlation;cosine;similarity measure;author cocitation analysis

    Dispelling the Myths Behind First-author Citation Counts

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    We conducted a full-scale evaluative citation analysis study of scholars in the XML research field to explore just how different from each other author rankings resulting from different citation counting methods actually are, and to demonstrate the capability of emerging data and tools on the Web in supporting more realistic citation counting methods. Our results contest some common arguments for the continued use of first-author citation counts in the evaluation of scholars, such as high correlations between author rankings by first-author citation counts and other citation counting methods, and high costs of using more realistic citation counting methods that are not well-supported by the ISI databases. It is argued that increasingly available digital full text research papers make it possible for citation analysis studies to go beyond what the ISI databases have directly supported and to employ more sophisticated methods

    Author Index

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    koamabayili/VECTRON-author-checklist: VECTRON author checklist

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    We have done our best to complete the author checklist relating to the use of animals in the hut study. Note that the objective for the hut study was to evaluate the IRS treatment applications for residual efficacy against Anopheles mosquitoes, including the local An. coluzzii mosquito population. Cows were only used to attract mosquitoes into the huts and no tests were carried out directly on the cows. The author checklist is intended for use with studies where experiments are carried out on animals, which is why we have had such difficulty in completing this for the hut study, as many of the questions do not relate to how the cows were used
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