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    Fracturation durant la production interne de fluides dans les roches : application à la migration primaire d'hydrocarbures

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    This thesis presents the experimental work and the results on fracturing of rock samples and analogue materials due to internal fluid generation during chemical reaction. The first two papers concentrate on time-resolved 3D X-ray imaging experiment on organic-rich shale samples. Paper 1 describes fracture formation due to hydrocarbon generation in the shale induced by organic matter decomposition during heating. Paper 2 gives an overview of the experimental procedure and image analysis workflow, which were used to obtain results presented in the first paper. The other two papers are focused on fracturing of gelatin mixed with yeast and sugar, which generates CO2. Paper 3 describes the mechanism of fracture network formation during draining of CO2 out of a gelatine layer. Paper 4 focuses on the temporal evolution of the drainage network and the mechanism of fracture opening and closing. The last paper presents a study in which X-ray microtomography was used to characterize porosity distribution in weathered andesite samples. The scientific methods developed in this project have potential application in studying dehydration of sediments, formation of mud volcanoes, methane hydrate exploration and assessment, geological sequestration of carbon dioxide CO2 and hydraulic fracturing of unconventional reservoirs.Cette thèse presente des travaux et résultats d'expériences de fracturation dont l'origine est une génération interne de fluides induite par des réactions chimiques dans des échantillons de roches et des matériaux analogues. Les deux premiers articles portent sur une expérience avec des échantillons de schistes imagés par tomographie aux rayons X au cours du temps. Le premier article décrit la formation de fractures créées par l'augmentation de pression induite par la décomposition de matière organique lorsque les schistes sont chauffés. Le deuxième article porte sur la procédure expérimentale et l'analyse d'images, utilisées pour obtenir les résultats du premier article. Les deux autres articles concernent la fracturation d'une couche de gélatine contenant de la levure et du sucre, ce qui génère du CO2. Le troisième article décrit le mécanisme de formation d'un réseau de fractures au cours du drainage du CO2 contenu dans la gélatine. Le quatrième article concerne l'évolution du réseau de fractures au cours de ce drainage, ainsi que les mécanismes d'ouverture et fermeture des fractures. Le dernier article porte sur une étude par tomographie aux rayons X de la distribution de porosité d'échantillons endommagés d'andésite. Les méthodes développées dans ce projet peuvent s'appliquer à la déshydratation de sédiments, la formation de volcans de boue, l'exploration d'hydrates de méthane, la séquestration de CO2 et la fracturation de réservoirs non conventionnels

    Fracturation durant la production interne de fluides dans les roches : application à la migration primaire d'hydrocarbures

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    This thesis presents the experimental work and the results on fracturing of rock samples and analogue materials due to internal fluid generation during chemical reaction. The first two papers concentrate on time-resolved 3D X-ray imaging experiment on organic-rich shale samples. Paper 1 describes fracture formation due to hydrocarbon generation in the shale induced by organic matter decomposition during heating. Paper 2 gives an overview of the experimental procedure and image analysis workflow, which were used to obtain results presented in the first paper. The other two papers are focused on fracturing of gelatin mixed with yeast and sugar, which generates CO2. Paper 3 describes the mechanism of fracture network formation during draining of CO2 out of a gelatine layer. Paper 4 focuses on the temporal evolution of the drainage network and the mechanism of fracture opening and closing. The last paper presents a study in which X-ray microtomography was used to characterize porosity distribution in weathered andesite samples. The scientific methods developed in this project have potential application in studying dehydration of sediments, formation of mud volcanoes, methane hydrate exploration and assessment, geological sequestration of carbon dioxide CO2 and hydraulic fracturing of unconventional reservoirs.Cette thèse presente des travaux et résultats d'expériences de fracturation dont l'origine est une génération interne de fluides induite par des réactions chimiques dans des échantillons de roches et des matériaux analogues. Les deux premiers articles portent sur une expérience avec des échantillons de schistes imagés par tomographie aux rayons X au cours du temps. Le premier article décrit la formation de fractures créées par l'augmentation de pression induite par la décomposition de matière organique lorsque les schistes sont chauffés. Le deuxième article porte sur la procédure expérimentale et l'analyse d'images, utilisées pour obtenir les résultats du premier article. Les deux autres articles concernent la fracturation d'une couche de gélatine contenant de la levure et du sucre, ce qui génère du CO2. Le troisième article décrit le mécanisme de formation d'un réseau de fractures au cours du drainage du CO2 contenu dans la gélatine. Le quatrième article concerne l'évolution du réseau de fractures au cours de ce drainage, ainsi que les mécanismes d'ouverture et fermeture des fractures. Le dernier article porte sur une étude par tomographie aux rayons X de la distribution de porosité d'échantillons endommagés d'andésite. Les méthodes développées dans ce projet peuvent s'appliquer à la déshydratation de sédiments, la formation de volcans de boue, l'exploration d'hydrates de méthane, la séquestration de CO2 et la fracturation de réservoirs non conventionnels

    Fracturing of tight rocks during internal fluid production: implications for primary migration

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    This thesis presents a study of fracture formation in low permeability rocks induced by generation of fluid or gas during chemical reaction. In nature, primary migration of hydrocarbons, i.e. generation of oil and gas from tight source rock and its expulsion to more permeable reservoirs, is driven by formation of microfractures in the heated organic-rich shale. The tomographic 3D imaging of the rocks samples during heating showed that micro-cracks develop in the shale due to internal pore pressure build-up. Generation of hydrocarbons drives fracture formation until a drainage network sufficient for expulsion is developed. Experiments were also conducted on analogue material, where gelatine was fractured during fermentation of yeast and sugar. Studies of the gel confined in Hele-Shaw cell showed that CO2 generation leads to formation of a drainage network which topology represents a new class of networks, intermediate between hierarchical fracture pattern and river\tree network. When CO2 escapes via fracture network, individual cracks open and close in intermittent manner. The variation of fracture opening in time exhibits a universal frequency distribution with 1/f and 1/f2 noise. These results have implication for understanding how the generated fluids escape from hydraulic fractures. The methods can be applied in studying dehydration of sediments, formation of mud volcanoes, methane hydrate exploration and assessment, geological sequestration of carbon dioxide CO2, hydraulic fracturing of unconventional reservoirs, hydrothermal energy

    Going Beyond Counting First Authors in Author Co-citation Analysis

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    The present study examines one of the fundamental aspects of author co-citation analysis (ACA) - the way co-citation counts are defined. Co-citation counting provides the data on which all subsequent statistical analyses and mappings are based, and we compare ACA results based on two different types of co-citation counting - the traditional type that only counts the first one among a cited work's authors on the one hand and a non-traditional type that takes into account the first 5 authors of a cited work on the other hand. Results indicate that the picture produced through this non-traditional author co-citation counting contains more coherent author groups and is therefore considerably clearer. However, this picture represents fewer specialties in the research field being studied than that produced through the traditional first-author co-citation counting when the same number of top-ranked authors is selected and analyzed. Reasons for these effects are discussed

    Variations on the Author

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    “Variations on the Author” discusses two of Eduardo Coutinho’s recent films (Um Dia na Vida, from 2010, and Últimas Conversas, posthumously released in 2015) and their contribution to the general question of documentary authorship. The director’s filmography is characterized by a consistent yet self-effacing form of authorial self-inscription: Coutinho often features as an interviewer that rather than express opinions propels discourses; an interviewer that is good at listening. This mode of self-inscription characterizes him as an author who is not expressive but who is nonetheless markedly present on the screen. In Um Dia na Vida, however, Coutinho is completely absent form the image, while Últimas Conversas, on the contrary, includes a confessional prologue that moves the director from the margins to the center of his films. This article examines the ways in which these works stand out in the filmography of a director who offers new insights into the notion of cinematic authorship

    Appropriate Similarity Measures for Author Cocitation Analysis

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    We provide a number of new insights into the methodological discussion about author cocitation analysis. We first argue that the use of the Pearson correlation for measuring the similarity between authors’ cocitation profiles is not very satisfactory. We then discuss what kind of similarity measures may be used as an alternative to the Pearson correlation. We consider three similarity measures in particular. One is the well-known cosine. The other two similarity measures have not been used before in the bibliometric literature. Finally, we show by means of an example that our findings have a high practical relevance.information science;Pearson correlation;cosine;similarity measure;author cocitation analysis

    Dispelling the Myths Behind First-author Citation Counts

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    We conducted a full-scale evaluative citation analysis study of scholars in the XML research field to explore just how different from each other author rankings resulting from different citation counting methods actually are, and to demonstrate the capability of emerging data and tools on the Web in supporting more realistic citation counting methods. Our results contest some common arguments for the continued use of first-author citation counts in the evaluation of scholars, such as high correlations between author rankings by first-author citation counts and other citation counting methods, and high costs of using more realistic citation counting methods that are not well-supported by the ISI databases. It is argued that increasingly available digital full text research papers make it possible for citation analysis studies to go beyond what the ISI databases have directly supported and to employ more sophisticated methods

    Author Index

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    koamabayili/VECTRON-author-checklist: VECTRON author checklist

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    We have done our best to complete the author checklist relating to the use of animals in the hut study. Note that the objective for the hut study was to evaluate the IRS treatment applications for residual efficacy against Anopheles mosquitoes, including the local An. coluzzii mosquito population. Cows were only used to attract mosquitoes into the huts and no tests were carried out directly on the cows. The author checklist is intended for use with studies where experiments are carried out on animals, which is why we have had such difficulty in completing this for the hut study, as many of the questions do not relate to how the cows were used
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