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Extraction behavior of Mo and W as homologs of Sg with α-benzoinoxime
Solvent extraction of molybdenum and tungsten as homologues of Sg with a-benzoinoxime from HCl solutions has been investigated. The extraction equilibration was achieved at 20s for Mo and W. Molybdenum was almost quantitatively extracted from 0.001 to 4M HCl solutions, and the extraction yields decreased at higher and lower acid concentrations due to the formation of anionic oxychloride complex and anionic species MO42-, respectively. The extraction yield of W was lower than that of Mo during the whole range of acid concentration. The composition of the extracted species was determined by using the slope method in present experiment. The elemental analysis, IR and 1H NMR spectra of the extracted species suggest that the extracted complex contain one MoO22+or WO22+ groups bonded with two a-benzoinoxime molecules
Study on Biosorption of Uranium by Rhodotorula Glutinis
Characteristic of uranium biosorption in water solution by Rhodotorula glutinis was investigated in the present study and the optimal pH for uranium adsorption was found to be 6-7.At the same time,maximum adsorption capacity of 149.4 mgU/(g dry cell)was identified,and Langmuir adsorption models can be used to simulate the isothermal biosorption process with high correlation coefficient of 0.99.According to Fourier transform infrared spectra,a new peak at wave number of 904 cm-1,which can be assigned to the ...中文摘要:研究了粘红酵母对水溶液中铀的吸附行为,发现其吸附铀的最佳pH值为6~7,最大吸附量为149.4mgU.g-1,其吸附等温线和Langmuir吸附等温方程符合较好,相关系数R2达到0.99;比较吸附铀前后粘红酵母的红外光谱图发现,吸附过铀的菌体的红外光谱在904cm-1处出现了一个新的峰,此峰为UO2的伸缩振动峰,说明粘红酵母确实对铀发生了吸附作用。此外,氨基或羟基的伸缩振动峰由3309移至3287cm-1,细胞壁中碳水化合物或醇中C—O键伸缩振动发生位移,由1068移至1080cm-1,说明这些基团可能参与了吸附过程;蛋白质的特征吸收峰(1653,1540,1237cm-1)在吸附前后基本无明显变化,表明粘红酵母的主要成分及结构仍保持完整。吸附后的菌体利用0.1mol.L-1的NaHCO3处理后可解吸出其中96%的铀,可见该菌在铀矿废水处理方面具有广阔的应用前景
A Quadruple Amplifier Rejected-Pile Up Used for High Counting Rate
A quadruple rejected-pile up amplifier used for high counting rate up to 105/s of average counting rate was described in this paper.To meet the need of high counting rate,the baseline regulation fuction,rejected pile up fuction was designed in the amplifier and the mark of rejected pile up was given for treatment of successive circuits.The quadruple amplifier consisting of four same circuits was assembled in one single NIM modul.These circuits have the advantages of compact construction,small volume and sta...中文文摘:介绍一种在高计数率情况下的反堆积放大器,它允许通过的平均计数为105/s。该放大器为了适应高计数率的要求,设计了基线调节功能和反堆积功能,给出了堆积标志,以便后继电路的处理。该电路在一个单宽NIM插件中有完全相同的四路电路工作,结构紧凑,体积小,工作性能稳定
Gettering of TiZrV Coatings on Pipe Inner-Walls of Vacuum System
采用直流磁控反溅射法在不锈钢真空管道内表面均匀镀上一层TiZrV薄膜。该薄膜经过激活后具有抽气效应,能够使真空管道由原来的系统气载转变成为管道泵。该薄膜激活温度很低,最低激活温度为180℃。在经过激活后,实验装置远端的真空度与泵口真空度相同,因此压力分布呈直线型。A novel technique was developed to turn the gas-load of the long,narrow stainless-steel pipes in vacuum system into non-evaporation getters (NEG).In the technique,the TiZrV films were grown by DC reactive magnetron sputtering on the inner walls of the pipes.The microstructures and compositions of the TiZrV coatings were characterized with scanning electron microscopy (SEM).The impacts of the activation conditions,including the activation temperature and time,on the gettering characteristics were studied.The results show that the TiZrV film,after activation at a lowest temperature of 180℃,is capable of gettering.The pressures at the remote end of the experimental setup and the pump inlet were found to be almost the same with a linear pressure distribution
一氧化氮参与调节UV-B诱导的豌豆幼苗生长抑制(英文)
对豌豆幼苗5天生长期内紫外线-B(UV-B)辐射对豌豆茎伸长生长和一氧化氮(NO)释放率的影响进行了研究.实验结果表明,UV-B辐射促进了豌豆茎中的NO释放,同时抑制豌豆茎伸长生长;外源NO供体根际处理豌豆幼苗,与UV-B辐射的上述效应相似;而用NO清除剂(PTIO)处理豌豆幼苗会产生和UV-B辐射相反的效应,即增加了茎的伸长.由此可推测,NO也许作为信号参与调节UV-B辐射诱导的生长抑制
127°径向位置灵敏柱形静电离子能谱仪
针对高电荷态离子与表面作用产生的溅射离子能谱测量,研制了一台127°径向位置灵敏柱形静电离子能谱仪。利用能量为800keV的Ar8+离子轰击金属铍靶产生的溅射离子测试了本谱仪。测试结果表明,该谱仪克服了传统静电谱仪通过扫描工作电压单能量点取谱的缺点,实现分段取谱——在单个工作电压下可同时获取一段0.85E≤E≤1.15E范围的能谱,从而提高测量效率
低剂量多次辐射对小鼠外周血淋巴细胞的影响
<正>为了评估低剂量多次辐射对健康机体产生的生物学风险,检测了X射线多次照射对BALB/c小鼠免疫系统的影响。采用X射线全身多次照射,第一天照射了0.07Gy
低能He~(2+)-He反应中单电子俘获微分散射过程的实验研究
利用冷靶反冲离子动量谱仪装置系统研究了20—40keVHe2+-He碰撞体系的态选择单电子俘获过程,实验获得了单电子俘获过程的态选择截面以及角微分截面.在所研究的能区范围,电子俘获到L壳层的截面最大,为主要的反应道,这与分子库仑过垒模型的反应窗理论的预测一致.实验测量的态选择截面与原子轨道紧耦合的计算结果很好地符合,与光谱方法的测量结果存在一定的差别,主要原因是光谱方法不能测量完整的反应通道信息.实验结果表明,总角微分截面在小角度范围主要来源于电子俘获到基态的贡献,在大角度范围主要来自电子俘获到激发态的贡献;电子俘获到基态的和激发态的角微分截面均出现振荡结构,这种振荡来源于电子俘获反应中分子轨道之间的相干效应.实验测量的角微分截面与其他实验和紧耦合方法的计算结果进行了比较和分析
HIRFL-CSR前端总线控制器的SD卡驱动
简要论述了用于兰州重离子加速器冷却储存环(HIRFL-CSR)控制系统的前端总线控制器。该控制器是基于ARM920T核心的AT91RM9200处理器,运行嵌入式Linux操作系统。描述了AT91RM9200处理器与Security Digital MemoryCard(SD卡)的硬件接口电路,分析了操作系统内核和Linux驱动程序结构,设计和实现了嵌入式Linux下基于AT91RM9200处理器的SD卡驱动程序
Multi-strip MRPCs for FOPI
During the last years FOPI has developed a new ToF system as an upgrade of the existing detector based on Multi-strip Multi-gap Resistive Plate Chambers (MMRPCs). The intention is to increase the charged Kaon identification up to a laboratory momentum of 1 GeV/c and to enhance the azimuthal detector granularity. The new ToF barrel has an active area of 5 m(2) with 2400 individual strips (900 x 1.6 mm(2)) [A. Schuttauf, et al., Nucl. Phys. B 158 (2006) 52] which are read out on both sides by a custom designed electronics [M. Ciobanu, et al., IEEE Trans. Nucl. Sci. NS-54 (4) (2007) 1201; K. Koch, et al., IEEE Trans. Nucl. Sci. NS-52(3) (2005) 745]. To reach the envisaged goal a time resolution of 100 ps is needed, at a flight path of 1-1.3 m. Due to the rare production of the K- at SIS energies the efficiency of the MMRPCs has to be above 95%. We report on measurements with the detectors and electronics from the mass production line. For this purpose we used a proton beam at 2.0 and 1.25 GeV, at rates between 0.1 and 5 kHz/cm(2) to determine the timing, efficiency and rate capability of the MMRPC