Chemotion-Repository
Not a member yet
22886 research outputs found
Sort by
distortionless enhancement with polarization transfer (DEPT) ()
No full textdataset for distortionless enhancement with polarization transfer (DEPT
13C nuclear magnetic resonance spectroscopy (13C NMR) ()
No full textdataset for 13C nuclear magnetic resonance spectroscopy (13C NMR)
13C NMR (100 MHz, Chloroform-d [77.0 ppm], ppm) δ = 163.3 (dd, J = 12.3 Hz, J = 251.2 Hz, 2C), 148.2, 146.5, 137.1, 137.2, 137.1, 129.4, 129.0 (2C), 128.8, 126.0 (2C), 117.5, 111.1 (dd, J = 7.7 Hz, J = 18.5 Hz, 2C), 104.7 (t, J = 25.0 Hz), 86.0, 56.3 (t, J = 1.9 Hz)
fast-atom bombardment mass spectrometry (FABMS) ()
No full textdataset for fast-atom bombardment mass spectrometry (FABMS)
MS (FAB, Matrix: 3-NBA): m/z (%) = 330 (21) [M+2H]+, 329 (100) [M+H]+, 328 (32) [M]+, 154 (15), 136 (11), 109 (39), 100 (14), 97 (15), 95 (13).HRMS–FAB (m/z): [M+H]+ Calcd for C17H22N6F, 329.1890; Found, 329.1889
heteronuclear single quantum coherence (HSQC) ()
No full textdataset for heteronuclear single quantum coherence (HSQC
heteronuclear single quantum coherence (HSQC) ()
No full textdataset for heteronuclear single quantum coherence (HSQC
infrared absorption spectroscopy (IR) ()
No full textdataset for infrared absorption spectroscopy (IR)
IR (ATR, ṽ) = 2972 (m), 2929 (w), 2867 (w), 2759 (w), 2720 (w), 2487 (w), 1605 (w), 1587 (w), 1548 (m), 1496 (w), 1468 (m), 1453 (s), 1424 (vs), 1401 (vs), 1378 (s), 1360 (vs), 1316 (s), 1242 (vs), 1213 (vs), 1156 (vs), 1119 (vs), 1103 (s), 1077 (m), 1041 (s), 1030 (m), 1014 (m), 977 (m), 958 (m), 908 (m), 878 (w), 841 (m), 776 (s), 731 (s), 711 (vs), 696 (s), 657 (m), 632 (w), 616 (w), 591 (m), 574 (m), 552 (s), 524 (m), 510 (m), 458 (m), 426 (w), 421 (w), 404 (w), 390 (w) cm–1
1H nuclear magnetic resonance spectroscopy (1H NMR) ()
No full textdataset for 1H nuclear magnetic resonance spectroscopy (1H NMR)
1H NMR (400 MHz, Chloroform-d [7.26 ppm], ppm) δ = 7.31–7.26 (m, 2H), 7.25–7.21 (m, 1H), 7.19–7.17 (m, 2H), 6.06 (d, J = 0.7 Hz, 1H), 5.40 (ps, 1H), 5.24 (s, 2H), 3.94 (ps, 1H), 2.16 (d, J = 0.6 Hz, 3H), 1.34 (ps, 6H), 1.21 (ps, 6H)
1H nuclear magnetic resonance spectroscopy (1H NMR) ()
No full textdataset for 1H nuclear magnetic resonance spectroscopy (1H NMR)
1H NMR (400 MHz, Chloroform-d [7.26 ppm], ppm) δ = 7.31–7.20 (m, 5H), 5.92 (s, 1H), 5.38 (s, 2H), 5.07–5.00 (m, 1H), 4.03–3.96 (m, 1H), 2.26 (s, 3H), 1.34 (d, J = 4.8 Hz, 6H), 1.21 (d, J = 5.3 Hz, 6H)
13C nuclear magnetic resonance spectroscopy (13C NMR) ()
No full textdataset for 13C nuclear magnetic resonance spectroscopy (13C NMR)
13C NMR (100 MHz, Chloroform-d [77.0 ppm], ppm) δ = 160.9 (Cq), 139.3 (Cq), 137.4 (Cq), 128.6 (CH, 2C), 127.3 (CH), 126.9 (CH, 2C), 93.6 (CH), 52.9 (CH2), 48.4 (CH), 45.4 (CH), 23.8 (CH3, 2C), 19.4 (CH3, 2C), 11.4 (CH3)