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Synthesis, Characterization and Textural Analysis of Functionalized Mesoporous Silica Using Sodium Silicate as Precursor and Silicone Surfactant as Template
Get PDFThree mesoporous silica with different functional group were prepared by one-step synthesis based on the simultaneous hydrolysis and condensation of sodium silicate with organo - silane in the presence of template surfactant polydimethylsiloxane - polyethyleneoxide (PDMS - PEO). The prepared materials were characterized by Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), atomic force microscopy (AFM) and nitrogen adsorption/desorption experiments. The results indicate that the preparation of methyl and phenyl functionalized silica were successful and the mass of methyl and phenyl groups bonded to the silica structure are 15, 38 mmol per gram silica. The average diameter of the silica particles are 103.51, 167.25 , and 86.41 nm while the average pore diameter are 6.7, 16.4, and 2.7 nm for unfunctionalized, methyl, and phenyl functionalized silica respectively
Synthesis and characterization of new Oxazine , Thiazine and Pyrazol derived from chalcones
Get PDFIn this study, chalcones were synthesis by condensing 2-acetylpyridine with aromatic aldehyde derivatives in dilute ethanolic potassium hydroxide solution at room temperature according to Claisen-Schmidt condensation. After that, new heterocyclic derivatives such as Oxazine, Thiazine and Pyrazol were synthesis by reaction between chalcones with urea, thiourea and hydrazine hydrate respectively scheme 1. All these compounds wrer characterization by FTIR, 1H-NMR spectroscopy and elemental analysis
Emission Spectra for the Isotopic Molecule Lithium Hydride
No full textA study of the emission spectra of isotopic for electronic states has been carried out. The energies of the vibration levels ( =0,1,..25) and the values of spectral lines R(J) and P(J) versus rotational quantum number (J=0,1..25). It was found that were an increase of the value of R(J) with the increase of the values of J was found while the value of P(J) decreases with decreasing of the values of J . It was found that corresponding to R(J) and P(J) the spectral line R(J) increases when the values of m increased
Biological activity and protease inhibitor from watery extract of lentil (Lens culinaris) against some bacterial species
No full textBiological activity substances was investigated in watery extract of lentil which found to contain phenols, tannin, saponins and resins while, flavons, terpens and steroids were not exist in the extract details explained that 5%, 10% of lentil extract largly inhibited the growth of Psedumonas aeruginosa then Escherichia coli and Bacillus subtilis. The growth of both Staphylococcus aureus and Salmonella typhimurium were slightly affected by all extract concentration. Extracellular protease were screened in all bacterial species under study. Complete inhibition was achieved for extracellular protease while different percentage of protease inhibition were seen for intracellular proteases
Efficacy of Saccharomyces cerevesiae on promoting growth in tomato
No full textThis study was conducted to evaluate the efficacy of Saccharomyces cerevesiae as a growth promoting agent in tomato. Soaking the seeds in yeast suspension at 5 g/L for 12h increased germination percentage, root length, root fresh and dry weight, plant height, foliage fresh and dry weight, attained 88.5% ; 8.1 cm ; 84.3 mg ; 7.03 mg ; 10.75 cm ; 839 mg and 37.75 mg compared with 80% ; 5.33 cm ; 39 mg ; 4.8 mg ; 7.35 cm ; 608 mg and 25.5 mg in seedlings grown from non treated seeds respectively. Similar results were obtained with seedling from seeds soaked in S. cerevesiae filtrate for 12 hrs. with values of 77.5% ; 6.875 cm ; 91.5 mg ; 7.5 mg ; 9.5 cm ; 777 mg and 40.35 mg compared to 66% ; 5.8 cm ; 57.7 mg ; 5.03 mg ; 5.9 cm ; 493 mg and 27.28 mg in control (non treated seeds) for the same above criteria respectively. Watering the soil together with spraying the foliar parts with S. cerevesiae suspension at 5 and 8 g/L were found to be more effective than watering and spraying the plants separately in plant growth stimulation under plastic house conditions. The leaf contents of chlorophyll attained to 60.4 and 61.17 SPAD unit compared with 50.37 SPAD units in control respectively and leaf area reached to 3124 and 3119 cm2 / plant compared with 1904 cm2 / plant in control for the two concentrations respectively. The treatment induced also an increasing in plant high ; fresh and dry weights which attained 222 cm ; 223.3 cm ; 1485.7 g ; 1489 g ; 340.7 g ; 341.7 compared to 186 cm ; 1169.3 g ; 286 g in control for the two concentrations respectively. Similar increasing in root length , root fresh and dry weight and yields which attained 30.33 cm ; 30.7 cm ; 61 g ; 61.33 g ; 14.33 g ; 14.33 g ; 6.9 kg / plant and 6.95 kg / plant compared to 24.13 cm ; 46 g ; 10 g and 4.22 kg / plant in control , were found. The stimulations of plant growth criteria was found in concomitance with increase of N ; P and K in treated plant leaves which reached 2.293 ; 2.3 ; 0.4007 ; 0.402 ; 0.5506 and 0.5723% compared to 1.458 ; 0.2283 and 0.1226% in control for the two concentrations respectively . In addition increasing in total solid soluble material (TSS), 5.2 and 5.2023% compared to 3.867% in control treatment were observed
Efficacy of Bacillus thuringiensis (Berliner) isolates on fig moth, Ephestia cautella (Walker) Larvae
No full textThe following dilution 5×10-1, 10-1, 10?2 , 10-3 gm/L for the indigenous isolate of Bacillus thuringiensis bacteria and the commercially isalate were used for experiments against the different stages of fig moth of E.cautella which exposed by filter paper method. The results showed that mortality of larval stages was increased with the increasing concentration of the biocide, in addition to increase in the mortality of the larval stages reached to the highest percentage in the third days of treatment of the larval stage in comparison with the first and second days of exposure. The results also showed that the sensitivity of larval stages was increased in first and second instars while reduced in the last instars .The high percentage of first instar mortality for the indigenous isolate in the concentration of 5×10-1 was 72.8% , while the low percentage of mortality showed in the concentration of 5×10-1 for the fifth instar larvae which was 13.3% in third days of treatment while a high percentage of mortality was showed for the first instar larvae for the commercially isulate in the concentration of 5×10-1 was 59.4% Furthermore, low percentage of mortality was shown in the concentration of 5×10-1 in fifth instar larval which was 8.3% in the third days of treatment. The results also showed that the indigenous isolated was more effective than the commercially produced bacteria for killing larval instars of fig moth E.cautella .The total percentage of larval instar mortality reached to 44.5 % after the third days of treatment in concentration 5×10-1 in the indigenous isolate , and it was 33.8 % in the commercially produced bacteria
The effect of Glycated Haemogloin A1c and Fasting Blood Glucose in Type1 Diabetes
Get PDFThe glycated haemoglobin A1c(HbA1c) and Fasting blood glucose(FBG) effect on type1 diabetic pateints as a screening tests and as a gold standard for assessing glycemic control in subjects with diabetes were studied .
Ninety one blood samples were collected in a peroid between June and the end of November 2012 at AL- Kindy Diabetic Center and Central Child Hospital,48 Females and 43 Males , aging between (11 month- 18 year), are divided into three groups, newly diagnosed , ongoing and healthy control group, with duration of disease between(1 day-3months) and (from birth-8 years) for newly diagnosed and ongoing groups respectevily .
The results showed that FBG and HbA1c for newly diagnosed were high (291 mmol/l and 10.6%) respectevily with short duration mean (3.32 week) while ongoing group (207mmol/L and 7.4%) with duration mean(154.5 week) compared with control group values (92.6mmol/L and 4.9%).There was a significant differences between FBG in patients and control at P value < 0.005, and p < 0.05 between HbA1c for patients and control .The correlation of FBG in patients and duration of disease were ( r= - ve 0.19) and for the control group ( r= -ve 0.49 ).When we compared FBG and HbA1c in patient the correlation was (+ve 0.64) .This study concluds that the combined use of FBG and HbA1c are very important for assessing glycemic control and enhanced the detection of diabetes individuals at high risk for diabetes
Studying the ability of transformation of lymphocytes by using PHA in patient with Cytomegalovirus
No full textBlood samples were collected from (31) pregnant women infected with cytomegalovirus , also (15) blood samples were collected from congenitally infected infants, and (20),(15),(15) blood samples were collected from pregnant women ,non pregnant and infants, respectively, all of them were as control groups.
CMV infection identified by using ELISA assay to detect specific CMV IgM & IgG in sera.
The results of lymphocyte transformation showed a significant decrease when phytoheamagglutinin (PHA) used as stimulator, lymphocytes response in infected pregnant women was lower than that of non infected pregnant women as well as non pregnant women. Result also showed a significant decrease in the ability of lymphocyte division in healthy pregnant women when compared with healthy non pregnant women. Lymphocyte activity of infants infected with CMV was also significally lower when comparison with non infected infants
The Electro-Excitation Form Factors for Low-Lying States of 7Li Nucleus
No full textThe transverse electron scattering form factors have been studied for low –lying excited states of 7Li nucleus. These states are specified by J? T= (0.478MeV), (4.63MeV) and (6.68MeV). The transitions to these states are taking place by both isoscalar and isovector components. These form factors have been analyzed in the framework of the multi-nucleon configuration mixing of harmonic oscillator shell model with size parameter brms=1.74fm. The universal two-body of Cohen-Kurath is used to generate the 1p-shell wave functions. The core polarization effects are included in the calculations through effective g-factors and resolved many discrepancies with experiments. A higher configuration effect outside the 1p-shell model space, such as the 2p-shell, enhances the form factors for q-values and reproduces the data. The present results are compared with other theoretical models.
PACS: 25.30.Bf Elastic electron scattering - 25.30.Dh Inelastic electron scattering to specific states – 21.60.Cs Shell model – 27.20. +n 5? A ?1
Synthesis, Characterization and Antimicrobial activity Study Via some new Schiff bases for Trimethoprim
No full textThis search reports the synthesis of some new series of Schiff base compounds for trimetheprim derivatives which known high been known as a medicinal effectiveness. Trimetheprim was condensed with several substituted aldehydes compounds.(4-dimethyl amine benzaldehyde , propanal , salicaldehyde, 2.4 dimethoxy benzaldehyde and 4- methyl benzaldehyde) to obtain Schiff base products(1a-5a) and several substituted ketones compound (4-aminoacetophenone,4-chloroacetophenone, isobutyleketone, acetylacetone and acetophenone) to obtain Schiff base products(6b-10b) in ethanol in the presence of concentrated sulphuric acid as a catalyst to yield the Schiff base. The structure of synthesized compounds has been established on the basis of their Chemical structures of all products were confirmed by spectrophotometric methods such as U.V. visible and FTIR.. All these compounds were evaluated for their antibacterial activity in vitro against Gram + ve bacteria (bacillus) , Gram –ve bacteria (E-Coli).Most Compound under investigation exhibited potent antibacterial activit