Revistas Universidad del Bío-Bío
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Influence of moisture content on the wave velocity to estimate the mechanical properties of large cross-section pieces for structural use of scots pine from spain
Full text linkThe aim of this research is to evaluate the influence of the moisture content of wood on stress wave velocity, as a nondestructive technique for estimating the mechanical properties of gross cross-section Spanish Scots pine (Pinus sylvestris) lumber for structural use. 26 100 x 150 x 3000 mm pieces from Segovia, Spain, were tested with different moisture content values, from 35,5 to 9%. Measurements of longitudinal stress wave velocity were carried out during the natural drying process by using three commercial portable devices based on ultrasonic, acoustic and vibrational techniques. The results can be summarized as three percentage points of decreasing velocity per percentage point of increased wood moisture content in the range from 11,8 to 21,4%: 0,48% for ultrasonic, 0,50% for acoustic wave and 0,65% for longitudinal vibration
Aplicación de celulosa nanofibrilada, en masa y superficie, a la pulpa mecánica de muela de piedra: Una sólida alternativa al tratamiento clásico de refinado
Full text linkSe ha estudiado el efecto de distintos dosajes en masa de nanofibras de celulosa (CNF ), comprendidas entre un 0 y un 6%, sobre las propiedades físico-mecánicas del papel obtenido a partir de las fibras de pasta mecánica de muela de piedra (SGW). Los resultados obtenidos se han comparado con el procedimiento convencional de refinado a distintos grados (de 0 a 2500 RPM). Posteriormente se ha estudiado la incidencia que tiene la aplicación superficial de las CNF en superficie, sobre el papel sin CNF en masa y con CNF en masa. Los resultados obtenidos mostraron que la rigidez del papel y su longitud de ruptura aumentaron con el grado de refino, sin embargo el grado Schopper – Riegler (ºSR) aumentó de forma importante dificultando el drenaje. La aportación de CNF en masa también aumentó el ºSR y la longitud de ruptura, de esta manera el ºSR de un refino a 1500 rev fue equivalente a un contenido en CNF de entre el 4,5 y 6%, pero su longitud de ruptura resultó ser sensiblemente superior. Puede concluirse que la aplicación de CNF en masa puede contemplarse como una alternativa al refino mecánico y que la aplicación superficial de CNF permite dotar al papel de mejores propiedades sin afectar a la capacidad de drenaje. AbstractThe effect of different application amounts of nanofibrilated cellulose (CNF), from 0 to 6%, on the physico-mechanical properties of the paper obtained from stone ground wood pulp fiber has been studied. The results have been compared with the conventional beating process at different degrees (from 0 to 2500 rpm). Afterwards the effect of the application of CNF on the surface, in papers with and without CNF in bulk, has been studied. The results showed that the paper stiffness and breaking length increased with freeness; however the Schopper–Riegler grade (oSR) increased significantly hindering drainage. The contribution of CNF in bulk also increased °SR and breaking length, therefore the °SR beaten at 1500 rev was equivalent to a content of CNF between 4,5 and 6%, but its breaking length was found to be substantially greater. It can be concluded that the CNF in bulk can be viewed as an alternative to mechanical beating and that the application of CNF at the paper surface allows increasing strength properties without affecting the drainage capacity
Influence of specimen orientation on determination of elesticity in static bending
Full text linkWood is a natural material and so many factors interfere in estimation of its physical and mechanical properties. Consequently variability in properties should be taken into account to rationalize its application. Longitudinal modulus of elasticity is one of the main mechanical properties of the material, and its value can be obtained via standardized tests. The aim of this study is to evaluate the influence of test conditions compatible with ABNT NBR 7190:1997 Code requirements to determine modulus of elasticity in static bending. For each of eight species, eight specimens were tested, all of them four times, with the sample oriented on each of its four faces related to load application. Data analysis was performed independently of species and their respective strength class, using hypothesis testing to evaluate influence of specimens’ orientations to determination. It was concluded that specimen orientation is significant in determining modulus of elasticity in static bending according to ABNT NBR 7190:1997. This aspect can lead to a future normative review by the National Committee responsible by redaction of this Code. To represent natural variability of wood in specimens’ volume by only one bending test, values of the modulus of elasticity should be lessened in 8%
Application of aqueous two phase systems based on polyethylene glycol and sodium citrate for the recovery of phenolic compounds from eucalyptus wood
Full text linkThis paper proposes an alternative way to intensify the exploitation of Eucalyptus wood wastes before valorisation for energy production. An aqueous two-phase system (ATPS) based on PEG 2000 and sodium citrate was investigated for the recovery of phenolic compounds that could act as natural antioxidants for applications including cosmetics, pharmaceuticals, food additives and other industrial applications. The influence of the tie line length (TLL) (26,1-46,1%), extraction temperature (25-65ºC), extraction time (90-390 min) and phase settlement time (1-8 h) were studied. Phenolic compounds were concentrated preferentially in the PEG-rich phase. A partition coefficient of 38 and a total phenols yield of 1,29 mg gallic acid equivalent/100 mg wood dry basis were obtained under the operational conditions selected: TLL, 46,1%, temperature 65ºC, extraction time 90 min and settlement time 1 h. Analysis of the extracts by RP-HPLC-ESI-TOF confirmed the presence of various phenolic compounds with demonstrated antioxidant activity: monogalloyl glucose, (-)-gallic acid, ellagic acid and quercetin 3-O-rhamnoside
The effect of moisture content on the retention and distribution of nano-titanium dioxide in the wood
Full text linkWhen chemically treating wood products is used to enhance the properties, the distribution of chemicals in the wood can be more important than the amount of chemical uptake. In this research, two moisture contents (MC) (0 and 25%) were used to study the effect of MC on the nanomaterial retention and distribution in cottonwood (Populus deltoides) sapwood treated with nano-titanium dioxide. The wood samples were impregnated by a full-cell process at three levels of nano-TiO2 concentration: 0,5; 1 and 1,5%. The nanomaterial retention was calculated and SEM images were used to investigate the distribution of nanoparticles in the wood. The results showed that increasing the nano-TiO2 concentration caused more retention and the MC difference caused almost identical retention at 0,5 and 1% concentrations. Although the retention in the 0% MC samples was slightly more than those of 25% MC, this retention was significantly more in these samples (0% MC) at 1,5% concentration. SEM images indicated that the nanoparticles had more uniform distribution in the 0% MC samples than the 25% MC ones and the difference was clearly visible at 1,5% concentration. Low MC ranges (about 0%) are better than high MC’s to impregnate cottonwood samples with nano-TiO2 by using the full-cell process
Treatability of Melia composita using vacuum pressure impregnation
Full text linkThe performance of treated wood in the field is ultimately affected by retention and penetration of preservative in wood. In the present study, a new preservative system ZiBOC and a commercially used preservative copper-chrome-arsenate (CCA) were used for evaluation of treatability of Melia composita by the vacuum pressure method at different pressure levels in unsealed and end sealed specimens. The retention and penetration levels of both the preservatives were significantly different at (P< 0.05) in sapwood, heartwood and pith zones. Melia composita exhibited treatability class ‘C’ (21 – 42% penetration). The results revealed that longitudinal penetration in Melia composita was the dominant flow as examined by spot test for copper in unsealed and end sealed specimens
Changes in the chemical structure and decay resistance of heat-treated narrow-leaved ash wood
Full text linkWe analyzed the effects of heat treatment on the chemical structure of wood from narrow-leafed Ash (Fraxinus angustifolia), a fast-growing and economically valuable species. We also analyzed the effects of heat treatment on the wood’s resistance to four decay fungi. Narrow-leafed Ash wood samples were heated with saturated steam to 140, 180, 200, and 220°C for 2, 4, and 6 h. The relative contents of extractable components were analyzed, as well as the levels of holocellulose, cellulose, and lignin. In addition, the density, equilibrium moisture content, and pH of the samples were measured. To determine the effects of heat treatment on resistance to decay fungi, the samples were exposed to the white rot fungus Trametes versicolor, dry rot fungus Serpula lacrymans, and the brown rot fungi Coniophora puteana and Gloeophyllum trabeum. Changes in the chemical composition of the wood due to heat treatment were correlated with increased resistance to fungal decay. While the hemicellulose content was dramatically reduced with increasing temperature and treatment duration, the lignin content increased proportionately. Thus, heat treatment is an environmentally friendly method of preserving narrow-leafed Ash wood against various decay fungi