Qucosa – Hemholtz-Zentrum Dresden-Rossendorf
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Infrared studies of impurity states and ultrafast carrier dynamics in semiconductor quantum structures
Get PDFThis thesis deals with infrared studies of impurity states, ultrafast carrier dynamics as well as coherent intersubband polarizations in semiconductor quantum structures such as quantum wells and superlattices, based on the GaAs/AlGaAs material system. In the first part it is shown that the 2pz confined impurity state of a semiconductor quantum well develops into an excited impurity band in the case of a superlattice. This is studied by following theoretically the transition from a single to a multiple quantum well or superlattice by exactly diagonalizing the three-dimensional Hamiltonian for a quantum well system with random impurities. Intersubband absorption experiments, which can be nearly perfectly reproduced by the theory, corroborate this interpretation, showing that at low temperatures in the low doping density regime all optical transitions originate from impurity transitions. These results also require reinterpretation of previous experimental data. The relaxation dynamics of interminiband transitions in doped GaAs/AlGaAs superlattices in the mid-IR are studied. This involves single-color pump-probe measurements to explore the dynamics at different wavelengths, which is performed with the Rossendorf freeelectron laser (FEL), providing picosecond pulses in a range from 3-200 µm and are used for the first time within this thesis. In these experiments, a fast bleaching of the interminiband transition is observed followed by thermalization and subsequent relaxation, whose time constants are determined to be 1-2 picoseconds. This is followed by an additional component due to carrier cooling in the lower miniband. In the second part, two-color pump-probe measurements are performed, involving the FEL as the pump source and a table-top broad-band tunable THz source for probing the transmission changes. These measurements allow a separate specification of the cooling times after a strong excitation, exhibiting time constants from 230 ps to 3 ps for different excitation densities and miniband widths. In addition, the dynamics of excited electrons within the minibands is explored and their contribution quantitatively extracted from the measurements. Intersubband absorption experiments of photoexcited carriers in single quantum well structures, measured directly in the time-domain, i.e. probing coherently the polarization between the first and the second subband, are presented. From the data we can directly extract the density and temperature dependence of the intersubband dephasing time between the two lowest subbands, ranging from 50 up to 400 fs. This all optical approach gives us the ability to tune the carrier concentration over an extremely wide range which is not accessible in a doped quantum well sample. By varying the carrier density, many-body effects such as the depolarization and their influence on the spectral position as well as on the lineshape on the intersubband dephasing are studied. Also the difference of excitonic and free-carrier type excitation is discussed, and indication of an excitonic intersubband transition is found
Experiments on upwards gas/liquid flow in vertical pipes
Get PDFTwo-phase flow experiments at vertical pipes are much suitable for studying the action of different constitutive relations characterizing the momentum exchange at the gas/liquid interface as well as the dynamic behaviour of the gas/liquid interface itself. The flow can be observed in its movement along the pipe and, in particular, within the shear field close to the pipe wall over a considerable vertical distance and, consequently, over a comparatively long time without the immediate separation of gas and liquid characteristic for horizontal flows. Wire-mesh sensors, which were the working horse in the described experiments, supplied sequences of instantaneous two-dimensional gas fraction distributions with a high-resolution in space and time. This allows to derive from the data not only void fraction and bubble velocity profiles, but also bubble size distributions, bubble-size resolved radial gas fraction profiles as well as the axial evolution of these distributions. An interfacial surface reconstruction algorithm was developed in order to extract the extension of interfacial area from the wire-mesh sensor data. The sensors were upgraded to withstand parameters that are close to nuclear reactor conditions. Most of the experiments were performed for both air/water flow at ambient pressure and steam/water flow of up to 6.5 MPa at identical combinations of the gas and liquid superficial velocities. This offers excellent conditions for studying the influence of the fluid properties
Turbulent dispersion of bubbles in poly-dispersed gas-liquid flows in a vertical pipe
Get PDFTurbulence dispersion is a phenomenon of practical importance in many multiphase flow systems. It has a strong effect on the distribution of the dispersed phase. Physically, this phenomenon is a result of interactions between individual particles of the dispersed phase and the continuous phase turbulence eddies. In a Lagrangian simulation, a particle-eddy interaction sub-model can be introduced and the effect of turbulence dispersion is automatically accounted for during particle tracking. Nevertheless, tracking of particleturbulence interaction is extremely expensive for the small time steps required. For this reason, the Lagrangian method is restricted to small-scale dilute flow problems. In contrast, the Eulerian approach based on the continuum modeling of the dispersed phase is more efficient for densely laden flows. In the Eulerian frame, the effect of turbulence dispersion appears as a turbulent diffusion term in the scalar transport equations and the so-called turbulent dispersion force in the momentum equations. The former vanishes if the Favre (mass-weighted) averaged velocity is adopted for the transport equation system. The latter is actually the total account of the turbulence effect on the interfacial forces. In many cases, only the fluctuating effect of the drag force is important. Therefore, many models available in the literature only consider the drag contribution. A new, more general derivation of the FAD (Favre Averaged Drag) model in the multi-fluid modeling framework is presented and validated in this report
Validation of the multiple velocity multiple size group (CFX10.0 N x M MUSIG) model for polydispersed multiphase flows
Get PDFTo simulate dispersed two-phase flows CFD tools for predicting the local particle number density and the size distribution are required. These quantities do not only have a significant effect on rates of mixing, heterogeneous chemical reaction rates or interfacial heat and mass transfers, but also a direct relevance to the hydrodynamics of the total system, such as the flow pattern and flow regime. The Multiple Size Group (MUSIG) model available in the commercial codes CFX-4 and CFX-5 was developed for this purpose. Mathematically, this model is based on the population balance method and the two-fluid modeling approach. The dispersed phase is divided into N size classes. In order to reduce the computational cost, all size groups are assumed to share the same velocity field. This model allows to use a sufficient number of particle size groups required for the coalescence and breakup calculation. Nevertheless, the assumption also restricts its applicability to homogeneous dispersed flows. We refer to the CFX MUSIG model mentioned above as the homogeneous model, which fails to predict the correct phase distribution when heterogeneous particle motion becomes important. In many flows the non-drag forces play an essential role with respect to the bubble motion. Especially, the lift force acting on large deformed bubbles, which is dominated by the asymmetrical wake, has a direction opposite to the shear induced lift force on a small bubble. This bubble separation cannot be predicted by the homogeneous MUSIG model. In order to overcome this shortcoming we developed an efficient inhomogeneous MUSIG model in cooperation with ANSYS CFX. A novel multiple velocity multiple size group model, which incorporates the population balance equation into the multi-fluid modeling framework, was proposed. The validation of this new model is discussed in this report
Construction and execution of experiments at the multi-purpose thermal hydraulic test facility TOPFLOW for generic investigations of two-phase flows and the development and validation of CFD codes - Final report
Get PDFThe works aimed at the further development and validation of models for CFD codes. For this reason, the new thermal-hydraulic test facility TOPFLOW was erected and equipped with wire-mesh sensors with high spatial and time resolution. Vertical test sections with nominal diameters of DN50 and DN200 operating with air-water as well as steam-water two-phase flows provided results on the evaluation of flow patterns, on the be¬haviour of the interfacial area as well as on interfacial momentum and heat transfer. The validation of the CFD-code for complex geometries was carried out using 3D void fraction and velocity distributions obtained in an experiment with an asymmetric obstacle in the large DN200 test section. With respect to free surface flows, stratified co- and counter-current flows as well as slug flows were studied in two horizontal test channels made from acrylic glass. Post-test calculations of these experiments succeeded in predicting the slug formation process. Corresponding to the main goal of the project, the experimental data was used for the model development. For vertical flows, the emphasis was put on lateral bubble forces (e.g. lift force). Different constitutive laws were tested using a Multi Bubble Size Class Test Solver that has been developed for this purpose. Basing on the results a generalized inhomogeneous Multiple Size Group (MUSIG) Model has been proposed and implemented into the CFD code CFX (ANSYS). Validation calculations with the new code resulted in the conclusion that particularly the models for bubble coalescence and fragmentation need further optimisation. Studies of single effects, like the assessment of turbulent dissipation in a bubbly flow and the analysis of trajectories of single bubbles near the wall, supplied other important results of the project
Experimental investigation and CFD simulation of slug flow in horizontal channels
Get PDFFor the investigation of stratified two-phase flow, two horizontal channels with rectangular cross-section were built at Forschungszentrum Dresden-Rossendorf (FZD). The channels allow the investigation of air/water co-current flows, especially the slug behaviour, at atmospheric pressure and room temperature. The test-sections are made of acrylic glass, so that optical techniques, like high-speed video observation or particle image velocimetry (PIV), can be applied for measurements. The rectangular cross-section was chosen to provide better observation possibilities. Moreover, dynamic pressure measurements were performed and synchronised with the high-speed camera system. CFD post-test simulations of stratified flows were performed using the code ANSYS CFX. The Euler-Euler two fluid model with the free surface option was applied on grids of minimum 4∙105 control volumes. The turbulence was modelled separately for each phase using the k-ω based shear stress transport (SST) turbulence model. The results compare well in terms of slug formation, velocity, and breaking. The qualitative agreement between calculation and experiment is encouraging and shows that CFD can be a useful tool in studying horizontal two-phase flow. Furthermore, CFD pre-test calculations were done to show the possibility of slug flow generation in a real geometry and at relevant parameters for nuclear reactor safety. The simulation was performed on a flat model representing the hot-leg of the German Konvoi-reactor, with water and saturated steam at 50 bar and 263.9°C. The results of the CFD-calculation show wave generation in the horizontal part of the hot-leg which grow to slugs in the region of the bend
Anwendung des Master Curve-Konzeptes zur Charakterisierung der Zähigkeit neutronenbestrahlter Reaktordruckbehälterstähle
Get PDFDie Anwendbarkeit des Master Curve-(MC-)Konzepts zur Charakterisierung des Zähigkeitszustandes bestrahlter Reaktordruck¬behälter-(RDB-)Stähle wurde an drei RDB-Stählen überprüft: IAEA-Referenzstahl 3JRQ57, 1JFL11 (vergleichbar mit 22NiMoCr3-7) sowie russischer WWER-440 Grundwerkstoff KAB-B. In Zugversuchen, Charpy-V-Tests, Risswiderstandskurven nach ASTM E1820 und Master Curve Tests zur Bestimmung der Referenztemperatur T0 nach ASTM E1921 wurden der unbestrahlte Ausgangszustand, je drei Bestrahlungszustände bis hin zu Neutronenfluenzen von 100∙10^18 n/cm² (E>1MeV) sowie bei 475°C/100h thermisch ausgeheilte Zustände untersucht. Mit zusätzlichen auf dem MC-Konzept basierenden Auswerteverfahren nach SINTAP, multimodalem MC-Ansatz (MML) sowie der Unified Curve erfolgte die Bewertung des Einflusses von Materialinhomogenitäten und möglicher MC-Formänderung bei hohen Fluenzen. Wie erwartet geht Neutronenbestrahlung mit Verfestigung und Duktilitätsabnahme einher, d.h. Härte, Festigkeitskennwerte, Charpy-V-Übergangstemperaturen T28J und T41J sowie T0 steigen mit der Neutronenfluenz, während die Bruchdehnung und Hochlagenzähigkeit abnehmen. Am bestrahlungsempfindlichsten reagiert der Stahl 3JRQ57, gefolgt von KAB-B und 1JFL11. Durch die Ausheilbehandlung von 475°C/100h erholen sich die Werkstoffkennwerte der Zugversuche, Charpy-V-Tests und MC-Versuche auf den jeweiligen unbestrahlten Ausgangszustand. Die technischen Ersatzkennwerte für duktile Rissinitiierung bleiben relativ unbeeinflusst von der Neutronenbestrahlung. Die MC nach ASTM E1921 beschreibt die Bruchzähigkeits-Temperaturverläufe für alle drei RDB-Stähle in allen Bestrahlungs- und Ausheilzuständen gut. Bei den niedrig und mittel bestrahlten Zuständen liegen meist mehr als 5% der KJc(1T)-Werte unterhalb der MC-Kurve für 5% Versagenswahrscheinlichkeit. Die MC beschreibt den hoch bestrahlte Zustand (ca. 100∙10^18 n/cm², E>1MeV) aller drei RDB-Stähle sehr gut, auch für Daten außerhalb des Gültigkeitsbereiches T0±50K, und auch für den bestrahlungsempfindlichen 3JRQ57 mit inhomogenem Gefüge. Die Unified Curve überbewertet den Einfluss der Neutronenbestrahlung auf die MC-Kurvenform. Eine mögliche Formänderung der MC durch Neutronenbestrahlung konnte bei keinem der drei untersuchten RDB-Stähle nachgewiesen werden