1,721,099 research outputs found

    Corrigendum to “Microstructure dependent dislocation density evolution in micro-macro rolled Al2O3/Al laminated composite” [Mater. Sci. Eng., A. 830 (7 January 2022) 142317] (Materials Science & Engineering A (2022) 830, (S0921509321015811), (10.1016/j.msea.2021.142317))

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    The authors regret that the original version of this publication contains some errors that should be corrected as follows: The affiliation of corresponding author (Catalin Iulian Pruncu) is incorrectly written. The correct affiliation should only read as: Departimento di Meccanica, Matematica e Management, Politecnico di Bari, Bari, 70125, Italy The authors offer their sincere apologies to the readers of the journal for any inconvenience caused

    Effects of process control agent amount, milling time, and annealing heat treatment on the microstructure of alcrcufeni high-entropy alloy synthesized through mechanical alloying

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    This study was conducted to investigate the characteristics of the AlCrCuFeNi high-en-tropy alloy (HEA) synthesized through mechanical alloying (MA). In addition, effects of Process Control Agent (PCA) amount and milling time were investigated using X-ray diffraction analysis (XRD), scanning electron microscopy (SEM), and energy dispersive X-ray spectroscopy (EDS). The results indicated that the synthesized AlCrCuFeNi alloy is a dual phase (FCC + BCC) HEA and the formation of the phases is strongly affected by the PCA amount. A high amount of PCA postponed the alloying process and prevented solid solution formation. Furthermore, with an increase in the PCA amount, lattice strain decreased, crystallite size increased, and the morphology of the mechanically alloyed particles changed from spherical to a plate-like shape. Additionally, investigation of thermal properties and annealing behavior at different temperatures revealed no phase transformation up to 400 °C; however, the amount of the phases changed. By increasing the temperature to 600 °C, a sigma phase (σ) and a B2-ordered solid solution formed; moreover, at 800 °C, the FCC phase decomposed into two different FCC phases

    Dynamic recrystallization nanoarchitectonics of FeCrCuMnNi multi-phase high entropy alloy

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    Dynamic recrystallization behavior of the FeCrCuMnNi high entropy alloy (HEA) was investigated through hot compression test at different temperatures and at constant strain rate. The results revealed that during hot deformation of FeCrCuMnNi HEA, flow stress and work hardening rate rapidly decreased with increasing the deformation temperature. Discontinuous dynamic recrystallization (dDRX) was found to be the main active mechanism during hot deformation, which was the governing mechanism even at higher temperatures. In addition, bulging was an effective mechanism for inducing new recrystallized nuclei. Grain growth was occurred at slow strain rate in comparison to conventional alloys and other HEAs. This behavior was attributed to the continuous nucleation during dDRX, sluggish diffusion, high solution hardening characteristics of HEAs, and the presence of multiple phases in the FeCrCuMnNi HEA. Texture analysis showed that at lower temperatures, deformation texture including // CA fiber was formed. By increasing the deformation temperature, the formation of recrystallization texture fibers such as // CA and // CA rapidly intensified

    Texture evolution and hardening behavior of Al/IF composite produced through severe plastic deformation

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    In this research, the microstructure, texture, and work hardening behavior of the Al/IF composite were investigated. The composites were produced through up to 7 cycles of accumulative roll bonding (ARB). The microstructure evolution revealed that the IF layer fractured during the process and distributed within the Al matrix due to its higher hardness and higher work hardening rate, as well as formation of shear bands. The main deformation textures formed in the Al layer were the {001} , {4,4,11} , and {111} components. In the IF layer, preferred orientations of {001} , {110} , and {111} were observed. The produced composite exhibited typical tensile behavior, with strength increasing and elongation decreasing during the process due to an increment in dislocation density and hardening. Additionally, the results revealed that the hardening capacity of the composite decreased during the process; however, the strain hardening rate increased. A noticeable increase in dislocation density and a decrease in crystallite size were found to be the main governing parameters of these variations. Moreover, the fracture mode of the composite changed from ductile fracture to a more brittle mode as a result of hardening

    Effect of composition and processing conditions on the direct reduction of iron oxide pellets

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    In this paper, HSC software is used to estimate the effects of composition and processing conditions on the reduction behavior of iron oxide pellets, i.e., hematite (Fe2O3), magnetite (Fe3O4), wustite (FeO), pure iron (Fe), and iron carbide (Fe3C), in a wide temperature range from room temperature (RT) to 1000°C in the presence of H2 and CO mixtures. The reducibility of iron ores, in particular Fe2O3, Fe3O4, FeO, Fe is discussed. The choice of reducing agents CO and H2 is explained, with CO proving to be the more effective reducing agent at high temperatures from a thermodynamic point of view. However, the free Gibbs energy of iron reduction is lowest in the presence of a 100% H2 atmosphere. In addition, H2 reduces tortuosity and increases porosity by reducing it at cooler temperatures and promoting diffusion. In contrast, CO increases tortuosity and reduces initial porosity because it requires higher temperatures for effective reduction and causes structural changes. The presence of impurities other than iron oxides has been shown to impair the activity of reduced pure iron by acting as catalyst poisons or participating in competing reactions. CaO accelerates the reduction of FeO, which is due to the formation of calcium ferrite, but the effect decreases at higher temperatures. MgO can either promote or hinder reduction, depending on its concentration and its influence on pellet porosity. The presence of several non‐iron oxides has been shown to affect the overall direct reduction of iron ore pellets, resulting in a significant impact of the overall process
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