8,440 research outputs found

    Mechanical characterization of metals by small sampling size

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    Classical plasticity models permit to simulate accurately the macroscopic response of several metals. This ability supports the development of indirect material characterization methodologies based on non-destructive testing, potentially applied for the fast integrity assessment of structural components in operating conditions. In this context, reducing the sampling size mitigates the invasiveness of the experiments and improves the manageability of portable equipment, although the representativeness of the information collected from small material volumes may become an issue. This contribution focuses on the equivalence between the mechanical properties that can be inferred from metal sampling of typical dimensions of hundreds or dozens microns, corresponding to indentation tests carried out at maximum load differing by one order of magnitude. This topic is addressed by the comparison of the results gathered from experimental and numerical analyses of pipeline steel

    On the non-isothermal precipitation of copper-rich phase in 17-4 PH stainless steel using dilatometric techniques

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    The kinetics of the precipitation of copper-rich phase in 17-4 PH stainless steel was studied in this paper by non-isothermal dilatometric experiments. The dilatometric curve was analyzed and the conversion degree of the precipitates was associated with the area under the derivative curve of the thermal expansion as a function of temperature. The apparent activation energy associated with the formation of the precipitates was calculated and the obtained results were compared with the data calculated from the isothermal dilatometric tests presented in a previous paper. The data well agree, so confirming that nonisothermal dilatometry can be considered a powerful method to study the precipitation kinetics of PH stainless steels. Finally, the conversion degree for any isothermal treatment was calculated starting from the parameters obtained by non-isothermal dilatometric tests and compared with the conversion degree calculated from the hardness values during heat treatments
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