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Essential oil composition of Terminalia ivorensis A. Chev. flowers from Northern Nigeria
Get PDFIn the present study, the volatile compounds identified in the essential oil from the flowers of Terminalia ivorensis A. Chev (Combretaceae) collected from Kaduna, Northern Nigeria, are reported. Essential oils were obtained using hydrodistllation in a Clevenger- type apparatus. The yield of the light yellow oil was found to be 0.22% (v/w, dry weight basis). The content and composition of the oil were analyzed by gas chromatography (GC-FID) and gas chromatography with electron impact mass spectrometry (GC-MS). The main compounds of the oil were δ-3-carene (29.4%) and α-pinene (20.9%). To the best of our knowledge, this is the first report on the essential oil constituents of any part of T. ivorensis
Essential oils of nigeria II: Analysis of the leaf oil of securidaca longependuculata fers
No full textAnti-inflammatory and anti-nociceptive activities of essential oil of Waltheria indica
Get PDFThis paper reports for the first time volatile compounds, anti-nociceptive and anti-inflammatory activities of essential oils from the leaves of Waltheria indica L. (Stericullaceae) growing in Nigeria. The essential oil was hydro-distilled and characterized by gas chromatography-flame ionization detection (GC-FID) and gas chromatography coupled with mass spectrometry (GC-MS) analyses. The anti-inflammatory activity was evaluated on carrageenan induced rat paw edema while the anti-nociceptive test was based on hot plate model. The hydro-distillation afforded 0.41% (dry weight basis) of light green oil. Forty compounds representing 99.8% were identified in the oil. The main constituents of the oil were limonene (34.7%), sabinene (21.2%) and citronellal (9.7%). The anti-nociceptive property of the essential oils statically inhibited edema development (p<0.001) at a dose of 200 and 400 mg/kg independent of time of exposure. However, the 100 mg/kg Waltheria indica essential oils (WIEO) displayed a relatively low inhibition (p<0.01-p>0.5) which declines as exposure time increases. The anti-inflammatory activities shows a steady rate and non-dose dependent activity (p<0.001) up to the 3rd h of inflammation study. Conversely, a sharp reduction at the rate of p<0.5, 0.1 and 0.01 for the 100, 200 and 400 mg/kg WIEO doses respectively. Overall, the results presented sustain and establish the anti-nociceptive and anti-inflammatory properties and justifies the need for further evaluation and development of the essential oils from this plant
In vivo anti-inflammatory and anti-nociceptive activities, and chemical constituents of essential oil from the leaf of Gardenia jasminoides J. Ellis (Rubiaceae)
Get PDFThe chemical constituents, anti-inflammatory and anti-nociceptive activities of the leaf essen-tial oil hydrodisitlled from the Gardenia jasminoides J. Ellis (Rubiaceae) were reported. The chemical constituents of the essential were analyzed using gas chromatography-flame ioniza-tion detector (GC-FID) and gas chromatography coupled with mass spectrometry (GC/MS). The hot plate and carrageenan-induced models were used to determine the anti-nociceptive and anti-inflammatory activities. The main compounds of the oil were pentadecanal 17 (49.2%), geranial 4 (12.3%), ar-turmerone 14 (8.2%) and 10-epi-γ-eudesmol 10 (6.2%). The essential oil of G. jasminoides at 100 and 400 mg.kg-1 doses significantly (p < 0.001) increased the latency period for the reaction duration in the anti-nociceptive study. The carrageenan-induced edema model reveals the suppression of inflammatory mediators (p < 0.001) within 1st, 2nd and 4th h for 100 mg.kg-1 dose, 1st and 4th h (200 mg.kg-1) and 1st-3rd h (400 mg.kg-1). The results indicate the potential of G. jasminoides essential oil as a source of pain relieving agent
Monoterpenoid constituents of the volatile oils of Cynometra megalophylla Harms., Caesalpinia pulcherrima L. Swartz and Pachylobus edulis G. Don., growing in Nigeria
No full textThe phytochemical investigation of the volatile oils from the root of Cynometra megalophylla Harms., the flower of Caesalpinia pulcherrima L. Swartz (Leguminosae) and the seeds of Pachylobus edulis G. Don (Burseraceae), by capillary gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS) are being reported. The investigation led to the identification of 43, 19 and 44 compounds in the oils of C. megalophylla, C. pulcherrima and P. edulis, respectively. While the oils of the former were highly dominated by monoterpenoids (86.8%), that of the latter were exclusively made up of monoteprenoids (98.8%). The major compounds of the oils were a-phellandrene (32.0% and 36.5%), p-cymene (18.2% and 15.3%) and g-terpinene (12.1% and 7.9%) in C. megalophylla and C. pulcherrima, respectively. However, a-pinene (13.7%), limonene (8.5%) and pentadecane (8.9%) constituted the bulk of the oil of P. edulis. It had 48.3% of monoterpenoids as well as 33.9% of straight-chain aliphatic hydrocarbon
Essential Oil of Phyllanthus reticulatus Poiret from Nigeria
Get PDFThe chemical composition of the essential oil obtained by hydrodistillation from the leaves of Phyllanthus reticulatus Poiret (Euphorbiaceae) growing in Nigeria has been studied. The constituents of the oil were analyzed by means of gas chromatography (GC-FID) and gas chromatography coupled with mass spectrometry (GC-MS). Monoterpenes (64.9%) were the dominant class of compounds, followed by sesquiterpenes (23.0%). The major constituents were α-pinene (6.0%), sabinene (7.6%), β-pinene (18.1%), linalool (6.9%) and camphor (7.7%), among the monoterpenes, and β-caryophyllene (11.9%) and germacrene D (8.6%) among the sesquiterpenes. This is
the first report on the volatile constituents of Phyllanthus reticulatu
Sesquiterpene-rich essential oil of Polyalthia longifolia Thw. (Annonaceae) from Nigeria
No full textThe essential oils of the leaf and stem bark of Polyalthia longifolia Thw. (Annonaceae) have been studied for their constituents by means of GC and GC/MS. The leaf oil was almost exclusively composed of sesquiterpene derivatives, being represented by allo-aromadendrene (19.7%), caryophyllene oxide (14.4%), β-caryophyllene (13.0%), β-selinene (7.9%), α-humulene (7.0%) and ar-curcumene (6.8%). However, α-copaene and α-muurolol (ca. 8.7%), β-selinene (8.6%), viridiflorene (8.1%), α-guaiene (7.8%), allo-aromadendrene (7.4%) and δ-cadinene (7.0%) were the major constituents occurring in the oil of the bark sample. All the other sesquiterpenoid compounds were observed in amount greater than 1%. α-Pinene (0.5%) and camphene (tr), which are the two monoterpenoids present in the leaf oil, could not be detected from the bark essential oi
Constituents of Cajanus cajan (L.) Millsp., Moringa oleifera Lam., Heliotropium indicum L. and Bidens pilosa L. from Nigeria
No full textThe essential oils of four plant species from Nigeria have been extracted by hydrodistillation and analyzed by GC and GC-MS. The oils of Cajanus cajan were comprised of sesquiterpenes (92.5%, 81.2% and 94.3% respectively in the leaves, stem and seeds). The major compounds identified were α-himachalene (9.0-11.5%), β-himachalene (8.0-11.0%), γ-himachalene (6.9-8.1%), a-humulene (7.1-8.7%) and α-copaene (4.5-5.6%). However, monoterpenoid compounds (81.8%) dominated the oil of Moringa oleifera with an abundance of α-phellandrene (25.2%) and p-cymene (24.9%). On the other hand, aldehydes (52.8%) occurred in the highest amount in Heliotropium indicum, represented by phenylacetaldehyde (22.2%), (E)-2-nonenal (8.3%) and (E, Z)-2-nonadienal (6.1%), with a significant quantity of hexahydrofarnesylacetone (8.4%). The leaf and stem oils of Bidens pilosa were dominated by sesquiterpenes (82.3% and 59.3%, respectively). The main compounds in the leaf oil were caryophyllene oxide (37.0%), β-caryophyllene (10.5%) and humulene oxide (6.0%), while the stem oils had an abundance of hexahydrofarnesyl acetone (13.4%), δ-cadinene (12.0%) and caryophyllene oxide (11.0%). The observed chemical patterns differ considerably from previous investigation
Essential oil constituents of Eclipta prostrata (L.) L. and Vernonia amygdalina Delile
No full textThe chemical composition of the essential oils from the leaves and stem bark of Eclipta prostrata (L.) L. and the aerial parts of Vernonia amygdalina Delile (Asteraceae) have been analyzed by capillary gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS). The investigation led to the identification of 33 and 30 compounds in the oils of the leaves and stem of E. prostrate, respectively, and 40 compounds in the oil of V. amygdalina. While the oil of the leaves of E. prostrata was highly dominated by sesquiterpenoids (89.3%), the stem bark was comprised of sesquiteprenoids (47.7%), straight chain hydrocarbons (25.6%) and monoterpenoids (11.1%). The main constituents of both oils were β-caryophyllene (47.7% and 15.9%) and α-humulene (31.8 and 12.9%) in the leaves and stem, respectively. In addition, (E)-β-farnesene (10.0%) was also identified in significant amount in the stem bark. On the other hand, the major component of V. amygdalina oil was α-muurolol (45.7%)
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