1,720,994 research outputs found
Tool life and surface integrity when turning titanium aluminides with PCD tools under conventional wet cutting and cryogenic cooling
No full textThe high-performance machining of difficult-to-cut alloys requires the development and optimization of high performance tools, able to withstand the thermo-mechanical tool load without compromising the surface quality of produced components. In this context, the machinability of titanium aluminides still represents a demanding challenge. In this paper, the performance of cubic boron nitride (CBN) and polycrystalline diamond (PCD) cutting inserts is compared to that of uncoated and coated carbide tools. Longitudinal external turning tests were performed on a Ti-43.5Al-4Nb-1Mo-0.1B (TNM) at.% cast and hot isostatically pressed (HIPed) γ-TiAl alloy, by using a conventional lubrication supply. In addition, PCD tools were also applied under cryogenic cooling with liquid nitrogen. Results proved that PCD cutting tools have the potential to improve the machining productivity of titanium aluminides, due to their high hardness and excellent thermal conductivity. A noteworthy further increase of tool life was possible by using PCD cutting inserts under cryogenic cooling condition
Environmental sustainability in the synthesis and characterization of hybrid/composite nanomaterials
Full text linkAlSiTiN and AlSiCrN multilayer coatings: Effects of structure and surface composition on tribological behavior under dry and lubricated conditions
No full textNanocomposite coatings have been widely studied over the last years because of their high potential in several applications. The increased interest for these coatings prompted the authors to study the tribological properties of two nanocomposites under dry and lubricated conditions (applying typical MQL media), in order to assess the influence of the surface and bulk properties on friction evolution. To this purpose, multilayer and nanocomposite AlSiTiN and AlSiCrN coatings were deposited onto tungsten carbide-cobalt (WC-Co) samples. Uncoated WC-Co materials were used as reference. Coatings were analyzed in terms of hardness and adhesion. The structure of the samples was assessed by X-ray diffraction (XRD), while the surface composition was studied by XPS analysis. Friction tests were carried out under both dry and lubricated conditions using an inox ball as counterpart. Both coatings showed high hardness and good adhesion to the substrate. As far as the friction properties are concerned, in dry conditions the surface properties affect the sliding contact at the early beginning, while bulk structure and tribolayer formation determine the main behavior. Only AlSiTiN coating shows a low and stable coefficient of friction (COF) under dry condition, while the use of MQL media results in a rapid stabilization of the COF for all the material
Surface treatment on an implant cobalt alloy for high biocompatibility and wear resistance
No full textAbstract Total hip prostheses are implanted to younger and more active patients, so the open problem is to create implants which will enhance the implant survivorship and will offer greater longevity. From this point of view, metal-on-metal arthroprostheses are well performing. The volume of periprosthetic inflammatory tissues appears to be less than with metal-on-UHMPWE, however osteolysis often occurs and it is known that the levels of metal ions in the blood and urine are elevated in patients with metal-on-metal bearing. The aim of this research activity was the synthesis and characterization of surface modified cobalt alloys, in order to obtain a biocompatible material presenting at the same time good wear performances, low metal ion release and low toxicity. The surface chemical composition of an implant cobalt alloy (Biodur) was modified, producing relevant tantalum enrichment. Tantalum was chosen because of its low toxicity and high corrosion resistance. The chemical composition, morphology, roughness, crystallographic structure and wettability of the surface, as well as the interface of the modified layer with the substrate, were characterized. The mechanical behavior of the modified materials was investigated by scratch and pin-on-disc wear tests. The metal ion release of the modified surfaces was measured by in vitro experiments after wear tests
Microstructural and spectrophotometric analysis system for metal welding processes
Full text linkWe describe an analysis system for some of the most important methods of metal welding, based on the acquisition, study and comparison of the atomic emission spectra (in the range from 250 nm to 830 nm), hyperspectral imaging between 600 nm and 950 nm wavelengths and microstructural analysis. The radiometric measurement system acquires information while the welding process is in progress and acquired data are then compared with those resulting from the subsequent microstructural analysis. It is known that the process parameters like, for example, the source power or its speed over the parts during welding, significantly affect the mechanical properties and quality of the resulting junction like hardness, porosity, presence of cracks or other damages and so on. On the other hand, these properties and, above all, the changes in the joint features due to unwanted variations in the process parameters or in the materials being welded, can be inferred by studying the microstructure. In this sense, a proper correlation between the in situ spectral analysis and the microstructural properties is of paramount importance for controlling and adjusting the parameters during the process. In line with the requirements of Industry 4.0, the system described is a study of the application of metrology in a production line, designed to increase information about the production parameters of mechanical industry without increasing costs and limiting the complexity of additional installations. In this paper we report a series of experiments performed using LASER and TIG welding systems applied to different metals. The comparison between the welding conditions acquired by the optical systems and the methods of structural analysis are the basis of a project to improve production systems and their automation
Study of the adhesive properties versus stability/aging of hernia repair meshes after deposition of RF activated plasma polymerized acrylic acid coating
Full text linkIn order to confer adhesive properties to commercial polypropylene (PP) meshes, a surface plasma-induced deposition of poly-(acrylic acid) (PPAA) is performed. Once biomaterials were functionalized, different postdeposition treatments (i.e. water washing and/or thermal treatments) were investigated with the aim of monitoring the coating degradation (and therefore the loss of adhesion) after 3 months of aging in both humid/oxidant (air) and inert (nitrogen) atmospheres. A wide physicochemical characterization was carried out in order to evaluate the functionalization effectiveness and the adhesive coating homogeneity by means of static water drop shape analysis and several spectroscopies (namely, FTIR, UV-Visible and X-ray Photoemission Spectroscopy). Themodification of the adhesion properties after post-deposition treatments aswell as aging under different storage atmospheres were investigated by means of Atomic Force Microscopy (AFM) used in Force/Distance (F/ D) mode. This technique confirms itself as a powerful tool for unveiling the surface adhesion capacity as well as the homogeneity of the functional coatings along the fibers. Results obtained evidenced that post-deposition treatments are mandatory in order to remove all oligomers produced during the plasma-treatment, whereas aging tests evidenced that these devices can be simply stored in presence of air for at least three months without a meaningful degradation of the original properties
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