39,762 research outputs found
3D characterisation of tool wear whilst diamond turning silicon
No full textNanometrically smooth infrared silicon optics can be manufactured by the diamond
turning process. Due to its relatively low density, silicon is an ideal optical
material for weight sensitive infrared (IR) applications. However, rapid diamond
tool edge degradation and the effect on the achieved surface have prevented
significant exploitation. With the aim of developing a process model to optimise
the diamond turning of silicon optics, a series of experimental trials were
devised using two ultra-precision diamond turning machines. Single crystal
silicon specimens (1 1 1) were repeatedly machined using diamond tools of the
same specification until the onset of surface brittle fracture. Two cutting
fluids were tested. The cutting forces were monitored and the wear morphology of
the tool edge was studied by scanning electron microscopy (SEM). The most
significant result showed the performance of one particular tool was
consistently superior when compared with other diamond tools of the same
specification. This remarkable tool performance resulted in doubling the cutting
distance exhibited by the other diamond tools. Another significant result was
associated with coolant type. In all cases, tool life was prolonged by as much
as 300% by using a specific fluid type. Further testing led to the development
of a novel method for assessing the progression of diamond tool wear. In this
technique, the diamond tools gradual recession profile is measured by performing
a series of plunging cuts. Tool shape changes used in conjunction with flank
wear SEM measurements enable the calculation of the volumetric tool wear rate.Wea
Diamond, L W, NX2320
No full textThis record was harvested from a previous catalogue system and will be withdrawn in 2025. Information in this record may be superseded or incomplete. Visit this record in UMA's new catalogue at: https://archives.library.unimelb.edu.au/nodes/view/381707Surname: DIAMOND. Given Name(s) or Initials: L W. Military Service Number or Last Known Location: NX2320. Missing, Wounded and Prisoner of War Enquiry Card Index Number: 5828.197775
Item: [2016.0049.14000] "Diamond, L W, NX2320
Argon plasma treatment techniques on steel and effects on diamond-like carbon structure and delamination
No full textCopyright © 2011 Elsevier B.V. All rights reserved.We demonstrate alteration in diamond-like carbon (DLC) film structure, chemistry and adhesion on steel, related to variation in the argon plasma pretreatment stage of plasma enhanced chemical vapour deposition. We relate these changes to the alteration in substrate structure, crystallinity and chemistry due to application of an argon plasma process with negative self bias up to 600 V. Adhesion of the DLC film to the substrate was assessed by examination of the spallated fraction of the film following controlled deformation. Films with no pretreatment step immediately delaminated. At 300 V pretreatment, the spallated fraction is 8.2%, reducing to 1.2% at 450 V and 0.02% at 600V. For bias voltages below 450V the adhesion enhancement is explained by a reduction in carbon contamination on the substrate surface, from 59at.% with no treatment to 26at.% at 450V, concurrently with a decrease in the surface roughness, Rq, from 31.5nm to 18.9nm. With a pretreatment bias voltage of 600V a nanocrystalline, nanostructured surface is formed, related to removal of chromium and relaxation of stress; X-ray diffraction indicates this phase is incipient at 450V. In addition to improving film adhesion, the nanotexturing of the substrate prior to film deposition results in a DLC film that shows an increase in sp3/sp2 ratio from 1.2 to 1.5, a reduction in surface roughness from 31nm to 21nm, and DLC nodular asperities with reduced diameter and increased uniformity of size and arrangement. These findings are consistent with the substrate alterations due to the plasma pretreatment resulting in limitation of surface diffusion in the growth process. This suggests that in addition to deposition phase processes, the parameters of the pretreatment process need to be considered when designing diamond-like carbon coatings.This work is partially supported by the Technology Strategy Board, reference BD266E
Investigation of the shape transferability of nanoscale multi-tip diamond tools in the diamond turning of nanostructures
No full textIn this article, the shape transferability of using nanoscale multi-tip diamond tools in the diamond turning for scale-up manufacturing of nanostructures has been demonstrated. Atomistic multi-tip diamond tool models were built with different tool geometries in terms of the difference in the tip cross-sectional shape, tip angle, and the feature of tool tip configuration, to determine their effect on the applied forces and the machined nano-groove geometries. The quality of machined nanostructures was characterized by the thickness of the deformed layers and the dimensional accuracy achieved. Simulation results show that diamond turning using nanoscale multi-tip tools offers tremendous shape transferability in machining nanostructures. Both periodic and non-periodic nano-grooves with different cross-sectional shapes can be successfully fabricated using the multi-tip tools. A hypothesis of minimum designed ratio of tool tip distance to tip base width (L/Wf) of the nanoscale multi-tip diamond tool for the high precision machining of nanostructures was proposed based on the analytical study of the quality of the nanostructures fabricated using different types of the multi-tip tools. Nanometric cutting trials using nanoscale multi-tip diamond tools (different in L/Wf) fabricated by focused ion beam (FIB) were then conducted to verify the hypothesis. The investigations done in this work imply the potential of using the nanoscale multi-tip diamond tool for the deterministic fabrication of period and non-periodic nanostructures, which opens up the feasibility of using the process as a versatile manufacturing technique in nanotechnology
Characterization of single-crystal synthetic diamond for multi-watt continuous-wave Raman lasers
No full textA continuous-wave diamond Raman laser is demonstrated with an output power of 5.1 W at 1217 nm. This Raman laser is intracavity pumped by a side-pumped Nd:YLF rod laser: a 43-fold brightness enhancement between the Nd:YLF and diamond Raman lasers is observed, with the M2 beam propagation factor of the diamond Raman laser measured to be <; 1.2. Although higher output powers are demonstrated in a similar configuration using KGd(WO4)2 (KGW) as the Raman laser material (6.1 W), the brightness enhancement is much lower (2.5 fold) due to the poorer beam quality of the KGW Raman laser (M2 <; 6). The Raman gain coefficient of single-crystal synthetic diamond at a pump wavelength of 1064-nm is also measured: a maximum value of 21±2 cm/GW is returned compared to 5.7±0.5 cm/GW for KGW at the same wavelength
Influence of temperature and crystal orientation on tool wear during single point diamond turning of silicon
No full textOwing to the capricious wear of cutting tools, ultra precision manufacturing of silicon through single point diamond turning (SPDT) operation becomes a challenging task. It thus becomes non-trivial to understand the contribution of temperature and crystal orientation during the SPDT process in order to suppress tool wear. Molecular dynamics (MD) simulation is an appropriate tool to study nanoscale processes occurring at the femtosecond/picosecond timescale which cannot otherwise be studied experimentally or by the finite element method (FEM). Accordingly, MD simulation has been deployed with a realistic analytical bond order potential (ABOP) formalism based potential energy function to simulate the single point diamond turning operation of single crystal silicon in order to understand the influence of temperature and crystal orientation on the tool wear mechanism. Results showed the strong influence of crystal orientation on the wear resistance of a diamond tool; cubic orientation performed better than dodecahedral orientation. It was also observed that high pressure phase transformation (HPPT) in the cutting zone was accompanied by the formation of dangling bonds of silicon. Under the influence of cutting temperature, the newly formed dangling bonds of silicon chemically combine with the pre-existing dangling bonds on the surface of the diamond tool resulting in the formation of silicon carbide (SiC), the main appearance of which was evident at the tool flank face. Continuous abrasion of the diamond cutting tool with SiC causes sp3–sp2 disorder of the diamond tool. Hence, both these processes proceed in tandem with each other. The mechanism proposed here is in good agreement with a recent experimental study, where silicon carbide and carbon like particles were observed using X-ray photoelectron spectroscope (XPS) technology after machining a silicon wafer with a diamond tool
Brittle–ductile transition during diamond turning of single crystal silicon carbide
No full textIn this experimental study, diamond turning of single crystal 6H-SiC was performed at a cutting speed of 1 m/s on an ultra-precision diamond turning machine (Moore Nanotech 350 UPL) to elucidate the microscopic origin of ductile-regime machining. Distilled water (pH value 7) was used as a preferred coolant during the course of machining in order to improve the tribological performance. A high magnification scanning electron microscope (SEM FIB- FEI Quanta 3D FEG) was used to examine the cutting tool before and after the machining. A surface finish of Ra=9.2 nm, better than any previously reported value on SiC was obtained. Also, tremendously high cutting resistance was offered by SiC resulting in the observation of significant wear marks on the cutting tool just after 1 km of cutting length. It was found out through a DXR Raman microscope that similar to other classical brittle materials (silicon, germanium, etc.) an occurrence of brittle-ductile transition is responsible for the ductile-regime machining of 6H-SiC. It has also been demonstrated that the structural phase transformations associated with the diamond turning of brittle materials which are normally considered as a prerequisite to ductile-regime machining, may not be observed during ductile-regime machining of polycrystalline materials
Magnetometry with nitrogen-vacancy defects in diamond
No full textThe isolated electronic spin system of the nitrogen-vacancy (NV) centre in diamond offers unique possibilities to be employed as a nanoscale sensor for detection and imaging of weak magnetic fields. Magnetic imaging with nanometric resolution and field detection capabilities in the nanotesla range are enabled by the atomic-size and exceptionally long spin-coherence times of this naturally occurring defect. The exciting perspectives that ensue from these characteristics have triggered vivid experimental activities in the emerging field of ‘NV magnetometry’. It is the purpose of this article to review the recent progress in high-sensitivity nanoscale NV magnetometry, generate an overview of the most pertinent results of the last years and highlight perspectives for future developments. We will present the physical principles that allow for magnetic field detection with NV centres and discuss first applications of NV magnetometers that have been demonstrated in the context of nano magnetism, mesoscopic physics and the life sciences
Seedless, Etchless Deposition of Nanocrystalline Diamond Coatings for Performance Improvements of Micro End Mills using Carbon Ion Implantation
No full textThis study compares the cutting performance of (1) as-received uncoated, (2) acid etched plus seeded plus nanocrystalline diamond (NCD) coated, (3) carbon ion implanted (CII) plus NCD coated, and (4) only CII micro end mills
Micro abrasive pencils with CVD diamond coating
No full textS.707-710Abrasive pencils (burs) for grinding can be made by coating cemented carbide bodies with a rough chemical vapour deposition (CVD) diamond layer. These tools have advantages compared to conventional abrasive pencils made by electroplating or sintering of diamond grains. Different CVD diamond abrasive pencils were manufactured with tip diameters ranging from 0.06 to 2.0 mm. A hot-filament CVD reactor was used in combination with a substrate holder system having a capacity of up to 240 tools. The grain size is the most important property of grinding tools. It must therefore be adjusted carefully in the coating process. The basic influence of tool geometry and coating parameters on the crystal size is presented. By prolonging the coating time to 90 h, crystal sizes of up to 50 m can be achieved. Manufacturing of abrasive pencils even with such long coating times can be economical, because thousands of tools could be coated in one process by industrial coating in bigger reactors. The relation between the crystal size and the roughness of ground workpieces is presented.1
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