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Fundiciones esferoidales austemperizadas con estructuras "Dual Phase": Microestructuras, tratamientos térmicos y propiedades mecánicas
No full textEn los últimos años, la atención de los investigadores en el área de ingeniería ha estado dirigida a la búsqueda de materiales que posean muy buenas propiedades mecánicas. En tal sentido, en el campo de las fundiciones de hierro se ha comenzado a estudiar recientemente un nuevo tipo de fundiciones con grafito esferoidal denominada Dual Phase, cuya microestructura está compuesta por ferrita alotriomórfica y ausferrita. La presente trabajo de investigación está centrado en el estudio de la obtención, y caracterización de la microestructura y de las propiedades mecánicas de este nuevo material. Entre los resultados reportados más significativos en el presente libro, se puede mencionar el desarrollo de dos metodologías para obtener microestructuras tipo Dual Phase utilizando diferentes ciclos térmicos. También se ha realizado un profundo estudio de las propiedades mecánicas. Finalmente, se desarrollaron estructuras Dual Phase con una morfología de fases controlada y totalmente novedosa. Este tipo de microestructura es absolutamente inédita, lo cual enriquece sustancialmente el conocimiento en el camino hacia la concreción industrial de estos materiales.Fil: Basso, Alejandro Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentin
Review on produccion processes and mechanical properties of dual phase austempered ductile iron
No full textDuring the last few years, researchers have sought new ductile iron (DI) applications focusing on the development of mixed microstructures, such as ferritic-bainitic or ferritic-martensitic. These kinds of structures result in DI with a good combination of mechanical properties, compared to other conventional DI. The combination of properties offered by the mixed structure DI, particularly in “dual phase austempered ductile iron” (ADI) has opened new horizons for cast iron to replace steel castings and forgings in many engineering applications. This new DI has a particular microstructure composed of different amounts and morphologies of ausferrite and free ferrite.
Dual phase ADI microstructures have afforded more opportunities for DI applications, acquiring better combinations of strength, ductility and toughness. This review describes the methodologies used to obtain this new kind of DI and the principal mechanical properties.Fil: Basso, Alejandro Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; ArgentinaFil: Sikora, Jorge Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingeniería; Argentin
Mechanical properties of a carbide-free bainitic cast steel with dispersed free ferrite
No full textA high silicon, medium carbon cast steel was designed and heat-treated in order to develop microstructures composed of carbide-free bainite and small amounts of free ferrite, with the aim of obtaining high strength cast steels with improved ductility. Because of microsegregation, it was observed that ferrite present in partially austenitised samples is mostly present at the highly alloyed zones, creating an interconnected network even for low proportions of this phase. Despite the coarse solidification structure and marked microsegregation in the cast steel, the mechanical properties obtained for both fully bainitic and bainitic-ferritic microstructures largely satisfy the minimum standard requirements for high strength cast steels and are similar to those reported for wrought steels of similar microstructures.Fil: Tenaglia, Nicolás Emanuel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Boeri, Roberto Enrique. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Basso, Alejandro Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentin
Wear behaviour of carbidic ductile iron with different matrices and carbide distribution
Get PDFJust like other properties, wear resistance is entirely dependent on materials microstructure, which, in turn, is related to the chemical composition and solidification rate that controls phases type, size, amount and dispersion. Depending on the tribosystem, the abrasive wear resistance of ductile iron (DI) may be improved by heat treatment as well as by reinforcing the matrix with hard particles like carbides, typically obtained by alloying with elements such as chromium. The solidification rate mainly depends on wall thickness and mould characteristics. In ductile iron, the solidification rate affects microstructural characteristics, such as nodule size, nodule count, carbide size and distribution and matrix refinement, also including the last to freeze (LTF) amount, size and distribution. This study evaluates the influence of the wall thickness (12.5, 25, 50 and 75 mm) on the abrasion resistance and impact toughness of DI with different matrices reinforced with carbides. Carbidic structures were obtained by alloying the melt with Cr; and the different types of matrices such us pearlitic, martensitic and ausferritc (CADI) were obtained under as cast conditions or by heat treatment. The results reflect the influence of cooling rate on the microstructural characteristics and its relationship with the mechanical properties, particularly the abrasive wear resistance. It was demonstrated that, under the present experimental conditions, the highest carbide content and matrix hardness, obtained from the 12.5 mm thick part with a martensitic matrix, resulted in the highest abrasion resistance.Fil: Basso, Alejandro Daniel. Universidad Nacional de Mar del Plata. Facultad de Ingenieria; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); ArgentinaFil: Laino, Sebastian. Universidad Nacional de Mar del Plata. Facultad de Ingenieria; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); ArgentinaFil: Dommarco, Ricardo. Universidad Nacional de Mar del Plata. Facultad de Ingenieria; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); Argentin
Influence of section size on dual phase ADI microstructure and properties: Comparison with fully ferritic and fully ausferritic matrices
Get PDFThe present work aims to evaluate and compare the influence that section size has on the microstructure and properties of fully ferritic, fully ausferritic and dual phase ADI matrices. Samples taken from 'Y' blocks of 25, 50 and 75 mm thickness were used to perform metallographic studies and mechanical tests. Cooling rate differences arising from changes in section size promote different microsegregation characteristics affecting solid state transformations and, consequently, the final microstructure and properties. When the section size increases, some properties decrease. The strongest deleterious effect was ascribed to the elongation and impact of ADI samples, where drops of nearly 40% were reached when specimens taken from the thinnest 'Y' blocks were compared to those taken from the thickest ones. Regarding fracture toughness, ferritic matrices exhibited the most noticeable detrimental effect. Dual phase ADI samples, on the other hand, presented the least deleterious section size effect on all the studied properties. © 2009 Institute of Materials, Minerals and Mining.Fil: Basso, Alejandro Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Martinez, Ricardo Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Sikora, Jorge Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentin
Development of high silicon dual phase austempered ductile iron
Get PDFThis work deals with the feasibility of obtaining Austempered Ductile Iron with Dual Phase structures (DPADI) through heat treatment, starting from different as-cast microstructures. The mechanical properties on these microstructures were evaluated. DPADI microstructures were obtained by adding different tenors of silicon (2.4% to 4.2%) to the melts and keeping the other alloying elements constant. The study focused on the determination of the time required to achieve the percentages of equilibrium phases (ferrite and austenite) at different temperatures in the intercritical temperature interval as a function of the starting as cast microstructure. The results showed that, as the silicon content increases, higher amount of ferrite is present in the as cast structure, and the time required to reach the thermodynamic equilibrium phases in the intercritical temperature interval is markedly reduced. Similarly, for a constant chemical composition, as the intercritical austenitizing temperature increases, the time required to reach the quantities of the equilibrium phases decreases. Regarding mechanical properties, the tests revealed that, as expected, as intercritical austenitising temperature increases so do tensile strength and hardness due to the higher ausferrite content in the DPADI matrix. These results indicate that high silicon Ductile Iron (with Si content higher than 3%) with a mostly ferritic microstructure in as cast conditions yields DPADI microstructures able to dispense with prior annealing heat treatments since the time required to reach the phase equilibrium percentages is compatible with the industrial practice and the mechanical properties are similar as compared to DPADI structures deriving from fully ferritic matrices.Fil: Basso, Alejandro Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); ArgentinaFil: Caldera, Martin. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingenieria; ArgentinaFil: Massone, Juan Miguel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); Argentina. Universidad Nacional de Mar del Plata. Facultad de Ingenieria; Argentin
Rolling contact fatigue behavior of dual-phase austempered ductile iron
Get PDFIn this work the rolling contact fatigue (RCF) behavior of dual-phase austempered ductile iron (ADI) was studied and compared to that of conventional ADI. The effect of surface finishing (manual vs. automatic grinding) on the surface properties and RCF endurance was also analyzed. RCF tests were performed in a flat washer type testing rig and using lubricated pure rolling conditions. RCF tests results were analyzed using the two-parameter Weibull distribution and the Weibayes method. The results indicated that the dual-phase ADI metal matrix was composed of 94% ausferrite and 6% free allotriomorphic ferrite, approximately. The hardness of conventional ADI was higher than that of dual-phase ADI. The residual stresses were compressive in all the cases with similar average values for ADI and dual-phase ADI. Relative to manual grinding, the automatic process increased slightly the surface hardness and reduced by around a 50% the residual stresses of both ADI and dual-phase ADI. Regarding RCF, failures were characterized by the typical concentrated damage in the form of spalls. No significant differences in the RCF endurance of ADI and dual-phase ADI were observed. No differences in the RCF endurance attributable to the surface finishing method were identified in the current tests.Fil: Colombo, Diego Alejandro. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Dommarco, Ricardo. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; ArgentinaFil: Basso, Alejandro Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones en Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones en Ciencia y Tecnología de Materiales; Argentin
Development and characterization of a new type of ductile iron with a novel multi-phase microstructure
Get PDFOver the last few years two new types of Ductile Iron (DI) have been developed based on Austempered DI (ADI), called Dual Phase ADI and Carbidic ADI (CADI), respectively. In the light of the experience acquired when studying these DI variants, the authors found motivating the possibility of obtaining a new type of multi-phase DI (MPDI), combining their main microstructural characteristics. A DI melt alloyed with 2%Cr, exhibiting free carbides and a pearlitic matrix in its as-cast condition, was used. The upper (UCT) and lower (LCT) critical temperatures of the Fe–C–Si equilibrium diagram region, where ferrite (α), austenite (γ) and graphite (Gr) coexist (called “intercritical interval”), were determined by heat treatment and microstructural analysis on samples previously annealed. Carbides stability was studied, and its dissolution was found to be negligible. It was possible to obtain free or allotriomorphic ferrite and austenite by isothermal austenitizing at temperatures within the intercritical interval, and then transform the remaining austenite into ausferrite after an austempering step. Therefore, multi- phase microstructures composed of graphite nodules, free carbides, free ferrite and ausferrite were obtained. The possibility of obtaining MPDI directly from the as-cast structure was also analyzed, and it was found that very similar microstructures to those previously annealed can be obtained by austenitizing samples at the same temperature range. These results proved that the pearlite → austenite transformation kinetics is rapid, as it took only one hour for the transformation to occur.Fil: Lagarde, Mayra. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones En Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones En Ciencia y Tecnología de Materiales; ArgentinaFil: Basso, Alejandro Daniel. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones En Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones En Ciencia y Tecnología de Materiales; ArgentinaFil: Dommarco, Ricardo. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones En Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones En Ciencia y Tecnología de Materiales; ArgentinaFil: Sikora, Jorge Antonio. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Mar del Plata. Instituto de Investigaciones En Ciencia y Tecnología de Materiales. Universidad Nacional de Mar del Plata. Facultad de Ingeniería. Instituto de Investigaciones En Ciencia y Tecnología de Materiales; Argentin
Analysis of mechanical properties and its associated fracture surfaces in dual-phase austempered ductile iron
Get PDFThis work aims at evaluating the fracture surfaces of tensile samples taken from a new kind of ductile iron referred to as ‘dual-phase Austempered Ductile Iron (ADI)’, a material composed of ausferrite (regular ADI microstructure) and free (or allotriomorphic) ferrite. The tensile fracture surface characteristics and tensile properties of eight dual-phase ADI microstructures, containing different relative quantities of ferrite and ausferrite, were studied in an alloyed ductile cast iron. Additionally, samples with fully ferritic and fully ausferritic (ADI) matrices were produced to be used as reference. Ferritic–pearlitic ductile irons (DI) were evaluated as well. For dual-phase ADI microstructures, when the amount of ausferrite increases, tensile strength, yield stress and hardness do so too. Interesting combinations of strength and elongation until failure were found. The mechanisms of fracture that characterise DI under static uniaxial loading at room temperature are nucleation, growth and coalescence of microvoids. The fracture surface of fully ferritic DI exhibited an irregular topography with dimples and large deformation of the nodular cavities, characteristic of ductile fracture. Microstructures with small percentages of ausferrite (less than 20%) yielded better mechanical properties in relation to fully ferritic matrices. These microstructures presented regions of quasi-cleavage fracture around last-to-freeze zones, related to the presence of ausferrite in those areas. As the amount of ausferrite increased, a decrease in nodular cavities deformation and a flatter fracture surface topography were noticed, which were ascribed to a higher amount of quasi-cleavage zones. By means of a special thermal cycle, microstructures with pearlitic matrices containing a continuous and well-defined net of allotriomorphic ferrite, located at the grain boundaries of recrystallised austenite, were obtained. The results of the mechanical tests leading to these microstructures revealed a significant enhancement of mechanical properties with respect to completely pearlitic matrices. The topographies of the fracture surfaces revealed a flat aspect and slightly or undeformed nodular cavities, as a result of high amount of pearlite. Still isolated dimple patterns associated to ferritic regions were observed.Fil: Basso, Alejandro Daniel. Universidad Nacional de Mar del Plata. Facultad de Ingenieria; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); ArgentinaFil: Martinez, Ricardo Antonio. Universidad Nacional de Mar del Plata. Facultad de Ingenieria; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); ArgentinaFil: Sikora, Jorge Antonio. Universidad Nacional de Mar del Plata. Facultad de Ingenieria; Argentina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Mar del Plata. Instituto de Investigación en Ciencia y Tecnología de Materiales (i); Argentin
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